5-己基-2-羟基-苯甲酸合成路线 (共 8 条)
反应条件
hydrogenchloride; sodium hydroxide in ethanol; water
参考文献
The Research Foundation of State University of New York
Patent: US4358443 A1, 1982 ;
反应条件
1: Zn, aq. HCl / 20 h / Heating 2: aq. NaOH / 12 h / Heating View Scheme
参考文献
Cox
Journal of the American Chemical Society, 1930 , vol. 52, p. 352,357
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Cox
Journal of the American Chemical Society, 1930 , vol. 52, p. 352,357
反应条件
1: 77 percent / aluminum chloride / CS2 / 12 h 2: Zn, aq. HCl / 20 h / Heating 3: aq. NaOH / 12 h / Heating View Scheme
参考文献
Coburn; Batista; Evans; Genco
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1245 - 1249
反应条件
1: 77 percent / aluminum chloride / CS2 / 12 h 2: Zn, aq. HCl / 20 h / Heating 3: aq. NaOH / 12 h / Heating View Scheme
参考文献
Coburn; Batista; Evans; Genco
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1245 - 1249
反应条件
1: aluminium chloride; carbon disulfide / Erhitzen des vom Schwefelkohlenstoff befreiten Reaktionsgemisches 2: aqueous KOH-solution 3: amalgamated zinc; aqueous hydrochloric acid View Scheme
参考文献
Cox
Journal of the American Chemical Society, 1930 , vol. 52, p. 352,357
反应条件
sodium hydroxide 12 h; Heating; Yield given;
参考文献
Coburn; Batista; Evans; Genco
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1245 - 1249
反应条件
1: PCl3 / chlorobenzene / 0.25 h / Heating
2: chlorobenzene / 3 h / Heating
View Scheme
参考文献
Coburn; Batista; Evans; Genco
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1245 - 1249