1,2:5,6-二-o-异亚丙基-alpha-d-ribo-3-己呋喃核糖合成路线 （共 32 条）
反应条件
dipyridinium dichromate; acetic anhydride in dichloromethane
参考文献
Silva, Sandrina; Sanchez-Fernandez, Elena M.; Ortiz Mellet, Carmen; Tatibouet, Arnaud; Pilar Rauter, Amelia; Rollin, Patrick
European Journal of Organic Chemistry, 2013 , # 35 p. 7941 - 7951
反应条件
3 A molecular sieve; pyridinium chlorochromate in dichloromethane 16 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Turks, Maris; Rodins, Vitalijs; Rolava, Evija; Ostrovskis, Pavels; Belyakov, Sergey
Carbohydrate Research, 2013 , vol. 375, p. 5 - 15
反应条件
1: With oxalyl dichloride; dimethyl sulfoxide in dichloromethane T=-70°C; 0.833333 h; 2: With triethylamine in dichloromethane T=-70°C; 0.5 h; 3: With water; ammonium chloride in dichloromethane T=-70 - 20°C;
参考文献
RANBAXY LABORATORIES LIMITED
Patent: WO2008/23336 A2, 2008 ;
Location in patent: Page/Page column 76 ;
WO 2008/023336 A2
反应条件
1: 68 percent / ZnCl2; aq. H3PO4 / 36 h / 20 °C 2: 91 percent / pyridinium dichromate; acetic anhydride / CH2Cl2 / 4 h / 75 °C View Scheme
参考文献
Hoffmann-Roeder, Anja; Johannes, Manuel
Chemical Communications, 2011 , vol. 47, # 35 p. 9903 - 9905
反应条件
chromium(VI) oxide; tert.-butylhydroperoxide in dichloromethane T=20°C; Oxidation; 12 h;
参考文献
Chandrasekhar; Mohanty, Pradyumna K.; Ramachander
Synlett, 1999 , # 7 p. 1063 - 1064
反应条件
acetic anhydride; pyridinium chlorochromate in dichloromethane 0.5 h; Ambient temperature;
参考文献
Soler, Tatiana; Bachki, Abderrazak; Falvello, Larry R.; Foubelo, Francisco; Yus, Miguel
Tetrahedron Asymmetry, 1998 , vol. 9, # 22 p. 3939 - 3943
反应条件
pyridinium chlorochromate
参考文献
Vangala, Madhuri; Dhokale, Snehal A.; Gawade, Rupesh L.; Pattuparambil, Rajamohanan R.; Puranik, Vedavati G.; Dhavale, Dilip D.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 40 p. 6874 - 6878
反应条件
in chloroform; water; isopropyl alcohol T=4°C; Cycloaddition; 48 h;
参考文献
Hall, Adrian; Bailey, Patrick D.; Rees, David C.; Rosair, Georgina M.; Wightman, Richard H.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 3 p. 329 - 343
反应条件
hydrogen; palladium on activated charcoal in methanol 18 h;
参考文献
Rosenthal, Alex; Cliff, Brian L.
Carbohydrate Research, 1980 , vol. 79, p. 63 - 78
反应条件
1: 32 percent / ZnCl2; H3PO4 / 30 h / 20 °C 2: 85 percent / PCC; 3 Angstroem molecular sieves; neutral alumina / CH2Cl2 / 15 h / 20 °C View Scheme
参考文献
Deshmukh, Abdul Rakeeb A. S.; Jayanthi, Arumugam; Thiagarajan, Kamanan; Puranik, Vedavati G.; Bhawal, Baburao M.
Synthesis, 2004 , # 18 p. 2965 - 2974
