N,N'-二苯基-1,2-苯二胺合成路线 （共 15 条）
反应条件
ammonium chloride; aniline; sodium t-butanolate; palladium diacetate in water; argon; toluene
参考文献
Patil, Abhimanyu O.; Habeeb, Jacob J.; Landis, Michael E.; Francisco, Manuel A.; Varma-Nair, Manika
Patent: US2007/265178 A1, 2007 ;
反应条件
bis(η3-allyl-μ-chloropalladium(II)); potassium tert-butylate; SIDip*HCl in 1,4-dioxane
T=100°C; 2 h; Inert atmosphere;
参考文献
Shen, Huafeng; Zhang, Zhong-Ping; Li, Jing-Hua
Journal of Chemical Research, 2010 , # 3 p. 163 - 166
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate in toluene
T=110°C; Inert atmosphereSchlenk technique; Reagent/catalystConcentrationSolvent;
参考文献
Wang, Han; Xia, Yuyu; Lv, Shang; Xu, Jingli; Sun, Zhihua
Tetrahedron Letters, 2013 , vol. 54, # 17 p. 2124 - 2127
反应条件
palladium diacetate; tri-tert-butyl phosphine; sodium t-butanolate in toluene
T=110°C; 14 h;
参考文献
Wenderski, Todd; Light, Kenneth M.; Ogrin, Doug; Bott, Simon G.; Harlan, C. Jeff
Tetrahedron Letters, 2004 , vol. 45, # 37 p. 6851 - 6853
反应条件
potassium hydroxide in ethanol
Hydrolysis; 2.5 h; Heating;
参考文献
Huang, Tian-Bao; Yu, Xiao-Ming; Liu, Lingfei; Wang, Ke
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 156, p. 9 - 20
反应条件
copper(l) iodide; potassium carbonate; L-proline in dimethyl sulfoxide
T=80°C; 18 h;
参考文献
Huang, Wen; Guo, Jianping; Xiao, Yuanjing; Zhu, Miaofen; Zou, Gang; Tang, Jie
Tetrahedron, 2005 , vol. 61, # 41 p. 9783 - 9790
反应条件
1: 24.5 percent / pyridine / Heating
2: 73.5 percent / 2 h / 300 °C
3: 70 percent / 50 percent aq. KOH / ethanol / 2.5 h / Heating
View Scheme
参考文献
Huang, Tian-Bao; Yu, Xiao-Ming; Liu, Lingfei; Wang, Ke
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 156, p. 9 - 20
反应条件
potassium hydroxide in ethanol
Deacetylation; 4.5 h; Heating;
参考文献
Chakrabarty; Batabyal; Khasnobis
Synthetic Communications, 2000 , vol. 30, # 20 p. 3651 - 3668
反应条件
1: K2CO3; Cu2I2 / 25 h / Heating
2: 2.0 g / aq. KOH / ethanol / 4.5 h / Heating
View Scheme
参考文献
Chakrabarty; Batabyal; Khasnobis
Synthetic Communications, 2000 , vol. 30, # 20 p. 3651 - 3668
反应条件
1: K2CO3; Cu2I2 / 25 h / Heating
2: 2.0 g / aq. KOH / ethanol / 4.5 h / Heating
View Scheme
参考文献
Chakrabarty; Batabyal; Khasnobis
Synthetic Communications, 2000 , vol. 30, # 20 p. 3651 - 3668
