1,4-二(硼酸基)-2-硝基苯合成路线 (共 2 条)
反应条件
sulfuric acid; nitric acid; acetic anhydride; urea T=-15°C; 3 h;
参考文献
Faury, Thomas; Dumur, Frederic; Clair, Sylvain; Abel, Mathieu; Porte, Louis; Gigmes, Didier
CrystEngComm, 2013 , vol. 15, # 11 p. 2067 - 2075
反应条件
1.1: magnesium; iodine / tetrahydrofuran / 20 h / |Inert atmosphere; |Reflux 1.2: -78 °C / |Inert atmosphere 2.1: water / water / |Inert atmosphere 3.1: nitric acid; sulfuric acid; urea; acetic anhydride / 3 h / -15 °C View Scheme
参考文献
Faury, Thomas; Dumur, Frederic; Clair, Sylvain; Abel, Mathieu; Porte, Louis; Gigmes, Didier
CrystEngComm, 2013 , vol. 15, # 11 p. 2067 - 2075