1,1’-磺酰双(3,4-二甲基苯)合成路线 （共 7 条）
参考文献
New Japan Chemical Co., Ltd.
Patent: US4778932 A1, 1988 ;
反应条件
trifluoromethylsulfonic anhydride; bis(N-methylpyridinium) sulfate 0.166667 h;
参考文献
Khodaei, Mohammad Mehdi; Nazari, Ehsan
Chemistry Letters, 2010 , vol. 39, # 4 p. 390 - 391
反应条件
trimethylsilyl chlorosulfonate T=80°C; 10 h;
参考文献
Hofmann, Karin; Simchen, Gerhard
Liebigs Annalen der Chemie, 1982 , # 2 p. 282 - 297
反应条件
SbF5; epoxysulfonyl fluoride T=0°C; 1 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Tanaka, Mutsuo; Souma, Yoshie
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3738 - 3740
反应条件
aluminium trichloride
参考文献
Horner,L.; Meyer,E.
Justus Liebigs Annalen der Chemie, 1975 , p. 2053 - 2078
反应条件
sulfur trioxide T=10 - 70°C; Product distribution;
参考文献
Moskvichev, Yu. A.; Sizyk, L. A.; Kramerova, S. K.; Mironov, G. S.
Journal of Organic Chemistry USSR (English Translation), 1982 , p. 118 - 122
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 1 p. 136 - 139
反应条件
sulfur trioxide other temperature, molar ratio of reagents, addition of acetic acid; multistep: 1) 30 deg C, 75 min. 2) 30 deg C, 45 min.; Product distributionMechanism;
参考文献
Moskvichev, Yu. A.; Shapiro, Yu E.; Kramerova, S. K.; Sizyk, L. A.; Shutova, I.V.; et al.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 284 - 289
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 2 p. 330 - 336
