N-[N-[N-[叔丁氧羰基]甘氨酰]甘氨酰]甘氨酸合成路线 (共 8 条)
反应条件
sodium hydrogencarbonate in water; N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Patel, Anupama; Lindhorst, Thisbe K.
Carbohydrate Research, 2006 , vol. 341, # 10 p. 1657 - 1668
反应条件
triethylamine in 1,4-dioxane; water; ethyl acetate
参考文献
NeoRx Corporation
Patent: US5541287 A1, 1996 ;
Title/Abstract Full Text Show Details
NeoRx Corporation
Patent: US6022966 A1, 2000 ;
反应条件
hydrogen; palladium on activated charcoal in methanol 2 h; Ambient temperature;
参考文献
Mack, Philip O. L.; Kelly, David P.; Martin, Roger F.; Wakelin, Laurence P. G.
Australian Journal of Chemistry, 1987 , vol. 40, # 1 p. 97 - 105
反应条件
sodium hydroxide in tetrahydrofuran; water; acetone
参考文献
Shering Corporation
Patent: US4169141 A1, 1979 ;
反应条件
1: 44 percent / diethyl phosphorocyanidate, Et3N / dimethylformamide / 1.) 0 deg C, 4 h, 2.) RT, 20 h 2: 74 percent / H2 / 5percent Pd/C / methanol / 2 h / Ambient temperature View Scheme
参考文献
Mack, Philip O. L.; Kelly, David P.; Martin, Roger F.; Wakelin, Laurence P. G.
Australian Journal of Chemistry, 1987 , vol. 40, # 1 p. 97 - 105
反应条件
in dimethyl sulfoxide T=20°C; 24 h;
参考文献
Gorokhova; Chinarev; Tuzikov; Tsygankova; Bovin
Russian Journal of Bioorganic Chemistry, 2006 , vol. 32, # 5 p. 420 - 428
反应条件
trifluoroacetic acid T=20°C; 2 h;
参考文献
Gorokhova; Chinarev; Tuzikov; Tsygankova; Bovin
Russian Journal of Bioorganic Chemistry, 2006 , vol. 32, # 5 p. 420 - 428
反应条件
1: 100 percent / CaCO3 / dimethylformamide / 1 h 2: trifluoroacetic acid / CH2Cl2 / 0.33 h / 20 °C View Scheme
参考文献
Fujii, Tomohiko; Manabe, Yoshiyuki; Sugimoto, Takanori; Ueda, Minoru
Tetrahedron, 2005 , vol. 61, # 33 p. 7874 - 7893