9,9-二甲基芴-2-甲酸合成路线 （共 4 条）
反应条件
sodium hypochlorite in methanol; water T=65 - 90°C; 3.5 h;
参考文献
HIROSE ENGINEERING CO., LTD.
Patent: EP1607392 A1, 2005 ;
Location in patent: Page/Page column 31 ;
反应条件
1: With potassium hydroxide in tetrahydrofuran; methanol 3 h; Reflux; 2: With hydrogenchloride in tetrahydrofuran; methanol; water pH=1;
参考文献
Li, Ming; Zeng, Hui; Meng, Yanyan; Sun, Huiqin; Liu, Song; Lu, Zhiyun; Huang, Yan; Pu, Xuemei
Dalton Transactions, 2011 , vol. 40, # 27 p. 7153 - 7164
反应条件
1: Br2 2: (i) Mg, BrCH2CH2Br, (ii) /BRN= 1900390/ View Scheme
参考文献
Li, Ming; Zeng, Hui; Meng, Yanyan; Sun, Huiqin; Liu, Song; Lu, Zhiyun; Huang, Yan; Pu, Xuemei
Dalton Transactions, 2011 , vol. 40, # 27 p. 7153 - 7164
反应条件
(i) Mg, BrCH2CH2Br, (ii) /BRN= 1900390/; Multistep reaction;
参考文献
Hallas,G. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1970 , p. 975 - 979
