4-乙酰基-5-氧己酸乙酯合成路线 （共 10 条）
反应条件
bis(acetylacetonate)nickel(II) T=160°C; 48 h;
参考文献
Nelson, John H.; Howells, Peter N.; DeLullo, George C.; Landen, George L.; Henry, Ronald A.
Journal of Organic Chemistry, 1980 , vol. 45, # 7 p. 1246 - 1249
反应条件
potassium carbonate T=37°C; 12 h;
参考文献
Shrout; Lightner
Synthesis, 1990 , # 11 p. 1062 - 1065
参考文献
March
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1902 , vol. 134, p. 180
Annales de Chimie (Cachan, France), 1902 , vol. <7> 26, p. 327,329
参考文献
Feofilaktow; Semenowa
Zhurnal Obshchei Khimii, 1953 , vol. 23, p. 450,458; engl. Ausg. S. 463, 470
反应条件
sodium acetate; acetic acid; zinc 2 h; Heating;
参考文献
Tetrahedron, , vol. 49, # 11 p. 2185 - 2200
反应条件
zinc; sodium nitrite 1) glac. CH3COOH, water, 0-14 deg C, 3 h, then room temp., overnight; 2) 65 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Journal of Heterocyclic Chemistry, , vol. 21, p. 139 - 144
参考文献
Journal of the Chemical Society, , p. 1430,1438
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 134, p. 180
Annales de Chimie (Cachan, France), , vol. <7> 26, p. 327,329
反应条件
sulfuric acid in tetrahydrofuran; water
T=20°C; 14 h;
参考文献
Unsworth, William P.; Coulthard, Graeme; Kitsiou, Christiana; Taylor, Richard J. K.
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1368 - 1376
反应条件
1: 1) NaNO2; 2) Zn / 1) glac. CH3COOH, water, 0-14 deg C, 3 h, then room temp., overnight; 2) 65 deg C, 5 h
2: 81.5 percent / aq. NaOH / ethanol / 2 h / Heating
View Scheme
参考文献
Shrout; Lightner
Synthesis, 1990 , # 11 p. 1062 - 1065
