4-氯苯甲醛 2-苯基腙合成路线 (共 15 条)
反应条件
C5H14NO(1+)*Cl(1-)*C2H2O4 in neat (no solvent) T=25 - 30°C; 0.00833333 h; Green chemistry;
参考文献
Yadav, Urmiladevi Narad; Shankarling, Ganapati Subray
Journal of Molecular Liquids, 2014 , vol. 191, p. 137 - 141
反应条件
iron (III) perchlorate in 1,2-dichloro-ethane T=20°C; 7 h;
参考文献
Oskooie, Hossien A.; Heravi, Majid M.; Sadnia, Akbar; Safarzadegan, Mehrak; Behbahani, Farahnaz K.
Mendeleev Communications, 2007 , vol. 17, # 3 p. 190 - 191
反应条件
1: 4-chloro-1-hydroxymethyl-benzene With chromium(VI) oxide; silica gel in tert-butyl alcohol 0.166667 h; 2: phenylhydrazine in tert-butyl alcohol 0.166667 h;
参考文献
Kiasat; Kazemi; Nourbakhsh
Synthetic Communications, 2005 , vol. 35, # 11 p. 1555 - 1558
反应条件
sodium acetate in ethanol; water T=20 - 80°C;
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
1: 80 percent / piperidine / ethanol / 3 h / Heating 2: ethanol / 3 h / Heating View Scheme
参考文献
Harb, Abdel-Fattah A.; Hesien, Abdel-Haleem M.; Metwally, Saoud A.; Elnagdi, Mohamed Hilmy
Liebigs Annalen der Chemie, 1989 , p. 585 - 588
反应条件
1.1: hydrogenchloride; sodium nitrite / water / 0.25 h / 0 °C 1.2: 0.5 h / 0 °C 2.1: sodium acetate / ethanol; water / 20 - 80 °C View Scheme
参考文献
Guru, Murali Mohan; Ali, Md Ashif; Punniyamurthy, Tharmalingam
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5295 - 5308
反应条件
in ethanol 3 h; Heating;
参考文献
Harb, Abdel-Fattah A.; Hesien, Abdel-Haleem M.; Metwally, Saoud A.; Elnagdi, Mohamed Hilmy
Liebigs Annalen der Chemie, 1989 , p. 585 - 588
反应条件
N-(dichloromethylene)-N,N-dimethylammonium chloride in 1,2-dichloro-ethane 1.) room temp., 1 h, 2.) reflux, 4 h;
参考文献
Kokel, Bruno; Menichi, Gabriel; Hubert-Habart, Michel
Synthesis, 1985 , # 2 p. 201 - 202
反应条件
selenium(IV) oxide in N,N-dimethyl-formamide T=100°C; 4 h;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 96, # 3 p. 219 - 224
反应条件
tert.-butylhydroperoxide; anhydrous iron chloride; oxygen; acetylacetone T=120°C; 6 h; Catalytic behavior; regioselective reaction;
参考文献
Panda, Niranjan; Jena, Ashis Kumar
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9401 - 9406,6
Title/Abstract Full Text Show Details
Panda, Niranjan; Jena, Ashis Kumar
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9401 - 9406