1,2-二甲基-4-苯基硫基苯合成路线 (共 8 条)
反应条件
tetra(n-butyl)ammonium hydroxide in water T=50°C; 24 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Xu, Hua-Jian; Liang, Yu-Feng; Zhou, Xin-Feng; Feng, Yi-Si
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 13 p. 2562 - 2568
反应条件
trifluorormethanesulfonic acid in dichloromethane 168 h; Reflux;
参考文献
Wada, Yasufumi; Otani, Kouji; Endo, Noriko; Kita, Yasuyuki; Fujioka, Hiromichi
Chemical Communications, 2010 , vol. 46, # 5 p. 797 - 799
反应条件
potassium hydroxide in N,N-dimethyl acetamide T=170 - 175°C;
参考文献
Campbell,J.R.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1830 - 1833
反应条件
sodium amide in ammonia 6 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Biehl, Edward R.; Razzuk, Aziz; Jovanovic, Misa V.; Khanapure, Subhash P.
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5157 - 5160
反应条件
sodium amide in ammonia 6 h; Yield given. Yields of byproduct given;
参考文献
Biehl, Edward R.; Razzuk, Aziz; Jovanovic, Misa V.; Khanapure, Subhash P.
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5157 - 5160
参考文献
Horner,L. et al.
Justus Liebigs Annalen der Chemie, 1968 , vol. 714, p. 91 - 111
参考文献
Voronkov,M.G. et al.
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, # 12 p. 2575 - 2584,2391 - 2399
参考文献
Bourgeois
Chemische Berichte, 1895 , vol. 28, p. 2319
Recueil des Travaux Chimiques des Pays-Bas, 1899 , vol. 18, p. 433