反应条件
1: 1.) diborane, 2.) 3 N NaOH, 30percent H2O2 / 1.) THF, RT, 1 h, 2.) 40 deg C, 1 h 2: 1.) pyridine, p-toluenesulfonyl chloride, 2.) H2 / platinum oxide / 1a ) 5 deg C, 0.5 h, b ) RT, 40 h, 2.) ethyl acetate, RT, 2 h View Scheme
参考文献
Takaishi, Naotake; Takahashi, Hitoshi; Yamashita, Osamu; Inamoto, Yoshiaki
Journal of Organic Chemistry, 1986 , vol. 51, # 25 p. 4862 - 4865
