2,6-二异丙基苯异氰酸酯合成路线 （共 27 条）
反应条件
tributylphosphine; di-isopropyl azodicarboxylate in dichloromethane T=-78 - 20°C; P=760 Torr;
参考文献
Journal of Organic Chemistry, , vol. 64, # 11 p. 3940 - 3946
反应条件
(NH4)2S2O8; copper diacetate; silver nitrate in dichloromethane; water T=40°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 17 p. 5430 - 5433
反应条件
triphenylphosphine in dichloromethane T=-78 - 20°C; P=760 Torr; Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 64, # 11 p. 3940 - 3946
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=25°C; 0.166667 h;
参考文献
Angewandte Chemie, , vol. 107, # 22 p. 2746 - 2749
反应条件
4-(N,N-dimethlyamino)pyridine in dimethyl sulfoxide T=70°C; carbonylation; 0.25 h;
参考文献
Journal of the American Chemical Society, , vol. 122, # 31 p. 7487 - 7493
反应条件
in tetrahydrofuran T=0 - 22°C; P=760.051 Torr; 3 h;
参考文献
Chemical Communications, , # 17 p. 1840 - 1841
反应条件
1: pyridine / CH2Cl2 / 1 h / 0 °C 2: KOH / methanol / 15 °C 3: 77 percent / (NH4)2S2O8 / AgNO3, Cu(OAc)2 / CH2Cl2; H2O / 2 h / 40 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 60, # 17 p. 5430 - 5433
反应条件
1: KOH / methanol / 15 °C 2: 77 percent / (NH4)2S2O8 / AgNO3, Cu(OAc)2 / CH2Cl2; H2O / 2 h / 40 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 60, # 17 p. 5430 - 5433
反应条件
in diethyl ether treatment of diethyl ether soln. of NiP(C(CH3)3)2CH2CH2P(C(CH3)3)2NC6H3(CH(CH3)2)2 with CO (1 atm, 22 °C) over 2 h; detd. by (1)H NMR, (13)C NMR, (19)F NMR, (31)P NMR, MAS;
参考文献
Chemical Communications, , # 17 p. 1840 - 1841
反应条件
sodium hydrogencarbonate in dichloromethane; water; toluene T=0 - 20°C;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 17, # 23 p. 8102 - 8112
