3-溴-2-羟基苯甲酸甲酯合成路线 (共 6 条)
参考文献
Hirwe; Patil
Proceedings - Indian Academy of Sciences, Section A, 1937 , vol. <A> 5, p. 321,322
反应条件
1: With toluene-4-sulfonic acid in water; acetonitrile
T=20°C; 0.0833333 h;
2: With N-bromosuccinmide in water; acetonitrile
T=20°C; 16 h; regioselective reaction;
参考文献
Bovonsombat, Pakorn; Ali, Rameez; Khan, Chiraphorn; Leykajarakul, Juthamard; Pla-On, Kawin; Aphimanchindakul, Suraj; Pungcharoenpong, Natchapon; Timsuea, Nisit; Arunrat, Anchalee; Punpongjareorn, Napat
Tetrahedron, 2010 , vol. 66, # 34 p. 6928 - 6935
反应条件
lithium hydroxide
T=20°C; 6 h;
参考文献
Dobler, Markus R.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 7 p. 963 - 964
反应条件
1.1: BCl3; AlCl3 / 1,2-dichloro-ethane / 4 h / 20 °C
1.2: 53 percent / aq. HCl / 1,2-dichloro-ethane / 0.17 h / 20 °C
2.1: 100 percent / aq. LiOH / 6 h / 20 °C
View Scheme
参考文献
Dobler, Markus R.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 7 p. 963 - 964
参考文献
Gilman; Stuckwisch
Journal of the American Chemical Society, 1943 , vol. 65, p. 1461,1463
参考文献
Hirwe; Patil
Proceedings - Indian Academy of Sciences, Section A, 1937 , vol. <A> 5, p. 321,322