噻吩-2-硫代羧酸 S-苯基酯合成路线 （共 10 条）
反应条件
dipotassium peroxodisulfate; tetraethylammonium bromide in 1,2-dichloro-ethane T=90°C; 40 h; Inert atmosphere;
参考文献
Zhu, Xuebin; Shi, Yan; Mao, Haibin; Cheng, Yixiang; Zhu, Chengjian
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3558 - 3562
反应条件
cesium fluoride in acetonitrile T=82°C;
参考文献
Shah, Syed Tasadaque Ali; Khan, Khalid Mohammed; Martinez Heinrich, Angelica; Voelter, Wolfgang
Tetrahedron Letters, 2002 , vol. 43, # 46 p. 8281 - 8283
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Shah, Syed T. A.; Khan, Khalid M.; Hussain, Hidayat; Hayat, Safdar; Voelter, Wolfgang
Monatshefte fur Chemie, 2005 , vol. 136, # 9 p. 1583 - 1589
反应条件
N,N-dicyclohexylmethylamine; sodium acetate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 in ethylene glycol dimethyl ether T=85°C; 18 h; chemoselective reaction;
参考文献
Burhardt, Mia N.; Taaning, Rolf H.; Skrydstrup, Troels
Organic Letters, 2013 , vol. 15, # 4 p. 948 - 951
反应条件
(Ph3P)2Pd(Ph)(I) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; P=760 Torr; 30 h;
参考文献
Gulevich, Yu. V.; Bumagin, N. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 10 p. 1918 - 1923
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 10 p. 2126 - 2132
反应条件
triethylamine; triphenylphosphine; palladium diacetate T=100°C; P=10343.2 Torr; 18 h;
参考文献
Cao, Hong; McNamee, Laura; Alper, Howard
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3530 - 3534
反应条件
hydroxymethanesulfinic acid sodium salt; cesium fluoride in water; N,N-dimethyl-formamide T=20°C; 0.5 h;
参考文献
Dan, Weixing; Deng, Hongjuan; Chen, Jiuxi; Liu, Miaochang; Ding, Jinchang; Wu, Huayue
Tetrahedron, 2010 , vol. 66, # 37 p. 7384 - 7388
反应条件
in chloroform T=20°C; 2 h;
参考文献
Pan, Xiangcheng; Curran, Dennis P.
Organic Letters, 2014 , vol. 16, # 10 p. 2728 - 2731
反应条件
1: bromodifluoromethyl phenyl sulphide With titanium tetrachloride in dichloromethane T=20°C; Friedel Crafts type alkylation; 0.25 h; Inert atmosphere; 2: thiophene in dichloromethane T=20°C; Friedel Crafts type alkylation; 2 h; Inert atmosphere;
参考文献
Kuhakarn, Chutima; Surapanich, Nakin; Kamtonwong, Siriporn; Pohmakotr, Manat; Reutrakul, Vichai
European Journal of Organic Chemistry, 2011 , # 29 p. 5911 - 5918
反应条件
dipotassium peroxodisulfate; tetraethylammonium bromide in 1,2-dichloro-ethane T=90°C; 40 h; Inert atmosphere;
参考文献
Zhu, Xuebin; Shi, Yan; Mao, Haibin; Cheng, Yixiang; Zhu, Chengjian
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3558 - 3562
反应条件
di-tert-butyl peroxide in neat (no solvent) T=120°C; 12 h; Inert atmosphereSchlenk technique;
参考文献
Zeng, Jing-Wen; Liu, Yi-Chen; Hsieh, Ping-An; Huang, Yu-Ting; Yi, Chih-Lun; Badsara, Satpal Singh; Lee, Chin-Fa
Green Chemistry, 2014 , vol. 16, # 5 p. 2644 - 2652
