4-(3-甲基-2-丁烯氧基)苯甲醛合成路线 （共 10 条）
反应条件
potassium carbonate in acetone T=20°C; 9 h;
参考文献
Suresh; Rajesh; Selvam; Venkateswarlu
Synthetic Communications, 2011 , vol. 41, # 7 p. 993 - 998
反应条件
potassium carbonate in acetone T=20°C;
参考文献
Liu, Zhiguo; Tang, Longguang; Zou, Peng; Zhang, Yali; Wang, Zhe; Fang, Qilu; Jiang, Lili; Chen, Gaozhi; Xu, Zheng; Zhang, Huajie; Liang, Guang
European Journal of Medicinal Chemistry, 2014 , vol. 74, p. 671 - 682
反应条件
1.1: 46 percent / potassium hydroxide / ethanol; H2O / 8 h / 20 °C 2.1: aq. HCl / methanol / 3 h / Heating 2.2: 37 percent / sodium acetate / methanol / 3 h View Scheme
参考文献
Kenez, Agnes; Juhasz, Laszlo; Antus, Sandor
Heterocyclic Communications, 2002 , vol. 8, # 6 p. 543 - 548
反应条件
1: 46 percent / potassium hydroxide / ethanol; H2O / 8 h / 20 °C 2: aq. HCl / methanol / Heating View Scheme
参考文献
Kenez, Agnes; Juhasz, Laszlo; Antus, Sandor
Heterocyclic Communications, 2002 , vol. 8, # 6 p. 543 - 548
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane T=20°C;
参考文献
Synthetic Communications, , vol. 43, # 1 p. 26 - 33
反应条件
potassium hydroxide in ethanol
参考文献
Taisho Pharmaceutical Co., Ltd.
Patent: US4085135 A1, 1978 ;
反应条件
1: N,N-diethylaniline / 20 h / 190 °C
2: potassium carbonate / acetone / 3 h / 20 °C
View Scheme
参考文献
Liu, Zhiguo; Tang, Longguang; Zou, Peng; Zhang, Yali; Wang, Zhe; Fang, Qilu; Jiang, Lili; Chen, Gaozhi; Xu, Zheng; Zhang, Huajie; Liang, Guang
European Journal of Medicinal Chemistry, 2014 , vol. 74, p. 671 - 682
反应条件
1: NaOEt / ethanol / -10 °C
2: toluene / Heating
View Scheme
参考文献
Moody, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 1333 - 1337
反应条件
hexacarbonyl molybdenum in toluene
T=110°C; 55 h;
参考文献
Bernard, Angela M.; Cocco, Maria T.; Onnis, Valentina; Piras, Pier P.
Synthesis, 1998 , # 3 p. 256 - 258
反应条件
N,N-diethylaniline
T=190°C; 20 h;
参考文献
Liu, Zhiguo; Tang, Longguang; Zou, Peng; Zhang, Yali; Wang, Zhe; Fang, Qilu; Jiang, Lili; Chen, Gaozhi; Xu, Zheng; Zhang, Huajie; Liang, Guang
European Journal of Medicinal Chemistry, 2014 , vol. 74, p. 671 - 682
