1-氯-4-(1-丙炔-1-基)苯合成路线 （共 11 条）
反应条件
tris[N-(tert-butyl)(3,5-dimethylphenyl)amido]molybdenum(VI) propylidyne; tris(2-hydroxy-5-nitro-benzyl)amine in tetrachloromethane T=20°C; 4 h; Inert atmosphere;
参考文献
Jyothish, Kuthanapillil; Zhang, Wei
Angewandte Chemie - International Edition, 2011 , vol. 50, # 15 p. 3435 - 3438
反应条件
(5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride; oxygen in hexane T=150°C; P=15001.5 Torr; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 78, # 11 p. 5691 - 5693
反应条件
(5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride; oxygen in hexane T=150°C; P=15001.5 Torr; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 78, # 11 p. 5691 - 5693
反应条件
bis(1,5-cyclooctadiene)nickel (0); water; caesium carbonate; tri-cyclo-hexyl-phosphine in toluene T=75°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 25 p. 5687 - 5690
反应条件
formic acid; Ru(O2CCF3)2(CO)(PPh3)2; tetra-(n-butyl)ammonium iodide in tetrahydrofuran T=95°C; 15 h; Inert atmosphere; regioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 25 p. 5687 - 5690
反应条件
1: With Ind2TiMe2 in toluene T=105°C; P=760 Torr; 7 h; 2: With sodium cyanoborohydride; zinc(II) chloride in methanol; toluene T=25°C; 16 h;
参考文献
Marcsekova, Klaudia; Wegener, Bernd; Doye, Sven
European Journal of Organic Chemistry, 2005 , # 22 p. 4843 - 4851
反应条件
C28H32MoO3Si in tetrachloromethane
T=40°C; 4.5 h; Inert atmosphere;
参考文献
The Regents of the University of Colorado, a body corporate; Zhang, Wei; Kuthanapillil, Jyothish; Wang, Qi
Patent: US2013/261295 A1, 2013 ;
Location in patent: Paragraph 0279; 0280 ;
反应条件
tris[N-(tert-butyl)(3,5-dimethylphenyl)amido]molybdenum(VI) propylidyne; tris(2-hydroxy-5-nitro-benzyl)amine in tetrachloromethane
T=20°C; 4 h; Inert atmosphere;
参考文献
Jyothish, Kuthanapillil; Zhang, Wei
Angewandte Chemie - International Edition, 2011 , vol. 50, # 15 p. 3435 - 3438
反应条件
dirhodium tetraacetate
参考文献
Domnin,I.N. et al.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 2144 - 2148
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, # 11 p. 2323 - 2327
反应条件
1: (i) Rh2(OAc)4, (ii) NaOH
View Scheme
参考文献
Domnin,I.N. et al.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 2144 - 2148
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, # 11 p. 2323 - 2327
