N-乙酰基-O-甲基-L-酪氨酸合成路线 （共 11 条）
反应条件
sodium hydroxide; acetic anhydride; dimethyl sulfate in water
参考文献
Richardson-Merrell Inc.
Patent: US4022910 A1, 1977 ;
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; C107H159NO9P2; hydrogen in methanol; cyclohexane T=20°C; P=45603.1 Torr; 2 h; Autoclave; optical yield given as percent eeenantioselective reaction;
参考文献
Yi, Bing; He, Hua-Ping; Fan, Qing-Hua
Journal of Molecular Catalysis A: Chemical, 2010 , vol. 315, # 1 p. 82 - 85
反应条件
sodium carbonate; sodium hydroxide in 1,4-dioxane; water T=0 - 20°C; 2 h;
参考文献
Beaufils, Damien; Danger, Gregoire; Boiteau, Laurent; Rossi, Jean-Christophe; Pascal, Robert
Chemical Communications, 2014 , vol. 50, # 23 p. 3100 - 3102
反应条件
[(S)-BINAPRuCl(benzene)]Cl; hydrogen in methanol T=20 - 50°C; P=3750.38 Torr; 12 h; AutoclaveInert atmosphere; Overall yield = 89.2 percent; enantioselective reaction;
参考文献
Arava, Veera Reddy; Amasa, Srinivasulu Reddy; Goud Bhatthula, Bharat Kumar; Kompella, Laxmi Srinivas; Matta, Venkata Prasad; Subha
Synthetic Communications, 2013 , vol. 43, # 21 p. 2892 - 2897
反应条件
water Behandeln des Reaktionsprodukts mit Dimethylsulfat und wss. Bariumhydroxid;
参考文献
Behr; Clarke
Journal of the American Chemical Society, 1932 , vol. 54, p. 1630,1633
参考文献
Guzow, Katarzyna; Ganzynkowicz, Robert; Rzeska, Alicja; Mrozek, Justyna; Szabelski, Mariusz; Karolczak, Jerzy; Liwo, Adam; Wiczk, Wieslaw
Journal of Physical Chemistry B, 2004 , vol. 108, # 12 p. 3879 - 3889
反应条件
1: water; acetone / 6 h / |Reflux 2: [(S)-BINAPRuCl(benzene)]Cl; hydrogen / methanol / 12 h / 20 - 50 °C / 3750.38 Torr / |Autoclave; |Inert atmosphere View Scheme
参考文献
Arava, Veera Reddy; Amasa, Srinivasulu Reddy; Goud Bhatthula, Bharat Kumar; Kompella, Laxmi Srinivas; Matta, Venkata Prasad; Subha
Synthetic Communications, 2013 , vol. 43, # 21 p. 2892 - 2897
反应条件
1: sodium acetate; acetic anhydride / 3.75 h / 40 - 135 °C 2: water; acetone / 6 h / |Reflux 3: [(S)-BINAPRuCl(benzene)]Cl; hydrogen / methanol / 12 h / 20 - 50 °C / 3750.38 Torr / |Autoclave; |Inert atmosphere View Scheme
参考文献
Arava, Veera Reddy; Amasa, Srinivasulu Reddy; Goud Bhatthula, Bharat Kumar; Kompella, Laxmi Srinivas; Matta, Venkata Prasad; Subha
Synthetic Communications, 2013 , vol. 43, # 21 p. 2892 - 2897
反应条件
sodium hydroxide; triphenylphosphine; diethylazodicarboxylate 1.) THF, 1 h; 2.) 10 min; Yield given. Multistep reaction;
参考文献
Krchnak, Viktor; Flegelova, Zuzka; Weichsel, Aleksandra S.; Lebl, Michal
Tetrahedron Letters, 1995 , vol. 36, # 35 p. 6193 - 6196
参考文献
Karrer
Helvetica Chimica Acta, 1922 , vol. 5, p. 478
