2,6,6-三甲基环己-2-烯-1-羧酸甲酯合成路线 （共 22 条）
反应条件
1: 83 percent / Mg / tetrahydrofuran / Heating
2: KH / hexamethylphosphoric acid triamide / 25 - 40 °C
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参考文献
Snowden, Roger L.; Linder, Simon M.; Muller, Bernard L.; Schulte, Karl H.
Helvetica Chimica Acta, 1987 , vol. 70, p. 1858 - 1878
反应条件
1: 81 percent / MCPBA / CH2Cl2 / 1.) 0 deg C, 2 h, 2.) r.t., 2 h
2: 70 percent / NaOMe / methanol / 10 h / Heating
3: 96 percent / CrO3, H2SO4 / acetone
4: 89 percent / NBS / CCl4 / Irradiation
5: 86 percent / NaOMe / methanol; tetrahydrofuran
6: 87 percent / K2CO3 / acetone
7: 51 percent / glac. AcOH, aq. HCl / 5 h / Heating
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参考文献
Kadas, Istvan; Arvai, Geza; Horyath, Gabriella
Organic Preparations and Procedures International, 1998 , vol. 30, # 1 p. 79 - 85
