4-氯-Alpha-苯基-苯甲胺合成路线 （共 12 条）
反应条件
1: 98 percent / TMSN3 / NaAuCl4 / CH2Cl2 / 16 h / 20 °C 2: LiAlH4 / tetrahydrofuran / 16 h / Heating View Scheme
参考文献
Terrasson, Vincent; Marque, Sylvain; Georgy, Marie; Campagne, Jean-Marc; Prim, Damien
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 15 p. 2063 - 2067
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 16 h; Heating;
参考文献
Terrasson, Vincent; Marque, Sylvain; Georgy, Marie; Campagne, Jean-Marc; Prim, Damien
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 15 p. 2063 - 2067
反应条件
Rink amine resin; water; trifluoroacetic acid; trimethyl orthoformate solid phase synthesis; 1) RT, 2) Et2O, toluene, 60 deg C, 24 h, 3) CH2Cl2, RT, 5 h; Yield given. Multistep reaction;
参考文献
Katritzky, Alan R.; Xie, Linghong; Zhang, Guifen; Griffith, Michael; Watson, Karen; Kiely, John S.
Tetrahedron Letters, 1997 , vol. 38, # 40 p. 7011 - 7014
反应条件
sodium amalgam; acetic acid
参考文献
Ingold; Wilson
Journal of the Chemical Society, 1933 , p. 1493,1503
Journal of the Chemical Society, 1934 , p. 93,97
反应条件
sodium amalgam; acetic acid
参考文献
Ingold; Wilson
Journal of the Chemical Society, 1933 , p. 1493,1503
Journal of the Chemical Society, 1934 , p. 93,97
反应条件
ammonium formate und Erhitzen des Reaktionsprodukts mit wss.HCl;
参考文献
Najer et al.
Bulletin de la Societe Chimique de France, 1959 , p. 352,355
反应条件
hydrogenchloride; borane-ammonia complex in aq. phosphate buffer T=37°C; pH=7.8;
参考文献
Ghislieri, Diego; Green, Anthony P.; Pontini, Marta; Willies, Simon C.; Rowles, Ian; Frank, Annika; Grogan, Gideon; Turner, Nicholas J.
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10863 - 10869
反应条件
hydrogenchloride; borane-ammonia complex in aq. phosphate buffer T=37°C; pH=7.8;
参考文献
Ghislieri, Diego; Green, Anthony P.; Pontini, Marta; Willies, Simon C.; Rowles, Ian; Frank, Annika; Grogan, Gideon; Turner, Nicholas J.
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10863 - 10869
反应条件
1.1: hydrogenchloride; borane-ammonia complex / aq. phosphate buffer / 37 °C / pH 7.8 2.1: N-ethyl-N,N-diisopropylamine / 4 h / 130 °C / |Inert atmosphere 3.1: sulfuric acid / methanol / 16 h / |Reflux 3.2: 2 h / pH 10 - 12 3.3: pH 4.5 View Scheme
参考文献
Ghislieri, Diego; Green, Anthony P.; Pontini, Marta; Willies, Simon C.; Rowles, Ian; Frank, Annika; Grogan, Gideon; Turner, Nicholas J.
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10863 - 10869
反应条件
hydrogenchloride; borane-ammonia complex in aq. phosphate buffer T=37°C; pH=7.8;
参考文献
Ghislieri, Diego; Green, Anthony P.; Pontini, Marta; Willies, Simon C.; Rowles, Ian; Frank, Annika; Grogan, Gideon; Turner, Nicholas J.
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10863 - 10869
