9-氮杂双环[3.3.1]壬烷合成路线 （共 8 条）
反应条件
hydrogen; palladium on activated charcoal; bis(η3-allyl-μ-chloropalladium(II)) in ethanol T=95°C; P=95000.1 Torr; 40 h;
参考文献
Hayashi, Tamio; Sawamura, Masaya; Ito, Yoshihiko
Tetrahedron, 1992 , vol. 48, # 11 p. 1999 - 2012
反应条件
1: With hydrazine T=80°C; Wolff-Kishner Reduction; 2 h; 2: With potassium hydroxide; 1,2-bis-(2-hydroxyethoxy)-ethane T=220°C; 0.5 h;
参考文献
Shibuya, Masatoshi; Tomizawa, Masaki; Sasano, Yusuke; Iwabuchi, Yoshiharu
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4619 - 4622
反应条件
1: 80 percent / 80percent N2H4*H2O, 85percent KOH / bis-(2-hydroxy-ethyl) ether 2: 67 percent / H2 / 10percent Pd/C, di-μ-chlorobis(π-allyl)dipalladium / ethanol / 40 h / 95 °C / 95000.1 Torr View Scheme
参考文献
Hayashi, Tamio; Sawamura, Masaya; Ito, Yoshihiko
Tetrahedron, 1992 , vol. 48, # 11 p. 1999 - 2012
反应条件
trimethylsilyl iodide in dichloromethane T=20°C; 12 h;
参考文献
Demizu, Yosuke; Shiigi, Hirofumi; Oda, Takahisa; Matsumura, Yoshihiro; Onomura, Osamu
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 48 - 52
反应条件
RuO4 in tetrachloromethane 3 h;
参考文献
Perrone; Carbonara; Tortorella
Archiv der Pharmazie, 1984 , vol. 317, # 7 p. 635 - 639
反应条件
phosphorus; hydrogen iodide T=260°C; im Rohr;
参考文献
Ciamician; Silber
Chemische Berichte, 1893 , vol. 26, p. 2750
Chemische Berichte, 1894 , vol. 27, p. 2851
Full Text Show Details
Ciamician; Silber
Gazzetta Chimica Italiana, 1894 , vol. 24 I, p. 135
Gazzetta Chimica Italiana, 1894 , vol. 24 II, p. 351
反应条件
Bei der Destillation des salzsauren Salzes;
参考文献
Ciamician; Silber
Gazzetta Chimica Italiana, 1894 , vol. 24 II, p. 354
Chemische Berichte, 1894 , vol. 27, p. 2853
反应条件
in dichloromethane
1.) 0 deg C, 1 h, 2.) room temperature, 12 h;
参考文献
Nelsen, Stephen F.; Kessel, Carl R.; Brien, David J.
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 702 - 711
