2-氮杂双环(2.2.2)辛烷合成路线 （共 7 条）
反应条件
hydrogen; sodium bis(2-methoxyethoxy)aluminium dihydride in toluene T=80 - 90°C; 2 h;
参考文献
Chung, John Y. L.; Ho, Guo-Jie
Synthetic Communications, 2002 , vol. 32, # 13 p. 1985 - 1995
反应条件
1: 89 percent / Dowtherm(R) A / 250 °C 2: 96.6 percent / H2 / Red-Al / toluene / 2 h / 80 - 90 °C View Scheme
参考文献
Chung, John Y. L.; Ho, Guo-Jie
Synthetic Communications, 2002 , vol. 32, # 13 p. 1985 - 1995
反应条件
1: 245 - 290 °C / Bei schnellem Erhitzen 2: sodium amide; toluene 3: lithium alanate; diethyl ether 4: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Werner; Ricca
Journal of the American Chemical Society, 1958 , vol. 80, p. 2733,2736
反应条件
palladium on activated charcoal; ethanol Hydrogenation;
参考文献
Werner; Ricca
Journal of the American Chemical Society, 1958 , vol. 80, p. 2733,2736
反应条件
1: lithium alanate; diethyl ether 2: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Werner; Ricca
Journal of the American Chemical Society, 1958 , vol. 80, p. 2733,2736
反应条件
1: 190 - 200 °C / Bei schnellem Erhitzen 2: sodium amide; toluene 3: lithium alanate; diethyl ether 4: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Werner; Ricca
Journal of the American Chemical Society, 1958 , vol. 80, p. 2733,2736
反应条件
acetic acid; sodium nitrite in water 50 h;
参考文献
Nelsen, Stephen F.; Gannett, Peter M.; Steffek, Daniel J.
Journal of Organic Chemistry, 1980 , vol. 45, # 19 p. 3857 - 3860
