1,1'-(1,2-乙炔二基)二(4-甲基苯)合成路线 （共 99 条）
参考文献
Harris
Journal of the American Chemical Society, 1930 , vol. 52, p. 3633
反应条件
ammonia; sodium amide
weiteres Reagens: Aether;
参考文献
Coleman; Holst; Maxwell
Journal of the American Chemical Society, 1936 , vol. 58, p. 2310
反应条件
Raney-Nickel W-2B in benzene
Heatingalso from other p-methyldithiobenzoic acid alkylesters;
参考文献
Latif, K. A.; Ali, M. Umar
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 5 p. 471 - 473
反应条件
pyridine in methanol
1 h;
参考文献
Kitamura, Tsugio; Muta, Tomonobu; Kobayashi, Shinjiro; Taniguchi, Hiroshi
Chemistry Letters, 1982 , p. 643 - 644
反应条件
potassium hydroxide in 1,4-dioxane
参考文献
Dombrovskii,A.V.; Taschchuk,K.G.
J. Gen. Chem. USSR (Engl. Transl.), 1963 , vol. 33, # 1 p. 165 - 170,158 - 162
反应条件
1: 43 percent / Br2 / CHCl3; CCl4 / 0 °C / Irradiation
2: 100 percent / NaN3, 1,4-diazabicyclo<2.2.2>octane / acetone / 2.5 h / Heating
3: 115 - 125 °C
View Scheme
参考文献
Neunhoeffer, Hans; Bopp, Ralf; Diehl, Werner
Liebigs Annalen der Chemie, 1993 , # 4 p. 367 - 374
反应条件
1: 100 percent / NaN3, 1,4-diazabicyclo<2.2.2>octane / acetone / 2.5 h / Heating
2: 115 - 125 °C
View Scheme
参考文献
Neunhoeffer, Hans; Bopp, Ralf; Diehl, Werner
Liebigs Annalen der Chemie, 1993 , # 4 p. 367 - 374
反应条件
1: 0.08 h / Heating
2: 33 percent / Raney-nickel W-2B / benzene / Heating; also from other p-methyldithiobenzoic acid alkylesters
View Scheme
参考文献
Latif, K. A.; Ali, M. Umar
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 5 p. 471 - 473
反应条件
1: CuCl2*2H2O / acetone
2: KOH / dioxane
View Scheme
参考文献
Dombrovskii,A.V.; Taschchuk,K.G.
J. Gen. Chem. USSR (Engl. Transl.), 1963 , vol. 33, # 1 p. 165 - 170,158 - 162
反应条件
1: CuCl2*2H2O / acetone
2: KOH / dioxane
View Scheme
参考文献
Dombrovskii,A.V.; Taschchuk,K.G.
J. Gen. Chem. USSR (Engl. Transl.), 1963 , vol. 33, # 1 p. 165 - 170,158 - 162
