1: 3-phenyl-propionyl chloride With triethylamine in dichloromethane
T=20°C; 16 h;
2: furan-2-yl-lithium in tetrahydrofuran
T=0°C; 1 h;
3: With hydrogenchloride in tetrahydrofuran
T=0°C; 0.25 h; Further stages.;
参考文献
Hansen, Anne-Lene L.; Murray, Anthony; Tanner, David
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 24 p. 4497 - 4505
hydrogenchloride; ammonium chloride
1.)1 h at 0 deg C and 12h at r.t., 2.)20 min. at -10 deg C, 3.)110 deg C at 0.1 Hgmm; Yield given. Multistep reaction;
参考文献
Van Royen; Mijngheer; De Clercq
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3283 - 3286
copper(l) iodide; oxygen
1.) hexane, THF, from -78 deg C to RT, 2.) CH2Cl2, RT, 10 h; Yield given. Multistep reaction;
参考文献
Lai, Long-Li; Shih, Li-Hua; Lin, Pen-Yuan; Wang, Jy-Shih; Shiao, Min-Jen
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1994 , vol. 41, # 1 p. 75 - 79
