(2,6-二甲氧基苯基)锂合成路线 （共 25 条）
参考文献
Justus Liebigs Annalen der Chemie, , vol. 709, p. 63 - 69
反应条件
n-butyllithium in hexane; pentane T=20°C;
参考文献
Journal of the American Chemical Society, , vol. 135, # 3 p. 1026 - 1036
反应条件
1: 1.6 g 3: 0.2 g / toluene-p-sulphonic acid / benzene / 72 h / Heating 4: 70 percent / bromine / acetic acid / 0.5 h 5: lithium carbonate / dimethylformamide 6: 2 g / 30percent hydrogen peroxide, potassium carbonate / acetone; H2O / 0 °C 7: 0.4 g / lithium aluminum hydride / diethyl ether / 5 h / Ambient temperature 8: periodic acid / methanol; H2O View Scheme
参考文献
Borthwick, Alan D.; Curry, David J.; Poynton, Alan; Whalley, W. Basil; Hooper, John W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2435 - 2444
参考文献
Khafagy,E.Z.; Lambooy,J.P.
Journal of Medicinal Chemistry, 1966 , vol. 9, p. 936 - 940
反应条件
TeCl4 in diethyl ether T=20°C; Substitution; 5 h;
参考文献
Asahara, Masahiro; Tanaka, Masahito; Erabi, Tatsuo; Wada, Masanori
Journal of the Chemical Society, Dalton Transactions, 2000 , # 20 p. 3493 - 3499
反应条件
1: 70 percent / diethyl ether / -30 °C 2: Na, NH3 / 4 h / -78 °C View Scheme
参考文献
Doorn, Johannes A. van; Meijboom, Nico
Recueil des Travaux Chimiques des Pays-Bas, 1992 , vol. 111, # 4 p. 170 - 177
参考文献
Kessler,H. et al.
Tetrahedron, 1969 , vol. 25, p. 287 - 293
反应条件
Sec-butyl alcohol in anhydrous butyl ether T=25°C; ΔH investigated; Thermodynamic data;
参考文献
Tetrahedron Letters, , vol. 27, # 20 p. 2247 - 2250
反应条件
2: aq. HBr / 170 °C View Scheme
参考文献
Khafagy,E.Z.; Lambooy,J.P.
Journal of Medicinal Chemistry, 1966 , vol. 9, p. 936 - 940
