4-乙基-2-甲氧基苯酚合成路线 （共 35 条）
反应条件
acetic acid; zinc T=70°C; 6 h; Reflux;
参考文献
Chittimalla, Santhosh Kumar; Bandi, Chennakesavulu; Putturu, Sireesha; Kuppusamy, Rajesh; Boellaard, Kevin Christopher; Tan, David Chu Aan; Lum, Demi Ming Jie
European Journal of Organic Chemistry, 2014 , vol. 2014, # 12 p. 2565 - 2575
反应条件
formic acid; ammonium formate; palladium 10 on activated carbon in water; ethyl acetate T=80°C; 3 h;
参考文献
SAMEC, Joseph; LUNDSTEDT, Anna; SAWADJOON, Supaporn; KAT2BIZ AB C/O INTERPARES KONSULT AB
Patent: WO2012/121659 A1, 2012 ;
Location in patent: Page/Page column 14 ;
反应条件
hydrogen in methanol T=20°C; 7 h;
参考文献
Monguchi, Yasunari; Fujita, Yuki; Endo, Koichi; Takao, Shinobu; Yoshimura, Masatoshi; Takagi, Yukio; Maegawa, Tomohiro; Sajiki, Hironao
Chemistry - A European Journal, 2009 , vol. 15, # 4 p. 834 - 837
反应条件
hydrogen T=325°C; P=124887 Torr; 0.7 h; Sealed tube;
参考文献
CHEMTEX ITALIA, S.P.A.; Elliott, Guliz Arf; Gastaldo, Dan; Murray, Aaron; Ryba, Steven
Patent: US2013/224816 A1, 2013 ;
Location in patent: Paragraph 0287-0293 ;
反应条件
hydrogen T=305°C; P=91809.2 Torr; 0.75 h; Sealed tube;
参考文献
CHEMTEX ITALIA, S.P.A.; Elliott, Guliz Arf; Gastaldo, Dan; Murray, Aaron; Ryba, Steven
Patent: US2013/224816 A1, 2013 ;
Location in patent: Paragraph 0287-0293 ;
反应条件
hydrogen T=325°C; P=124887 Torr; 1.16667 h; Sealed tube;
参考文献
CHEMTEX ITALIA, S.P.A.; Elliott, Guliz Arf; Gastaldo, Dan; Murray, Aaron; Ryba, Steven
Patent: US2013/224816 A1, 2013 ;
Location in patent: Paragraph 0287-0293 ;
反应条件
hydrogen T=325°C; P=124887 Torr; 1.16667 h; Sealed tube;
参考文献
CHEMTEX ITALIA, S.P.A.; Elliott, Guliz Arf; Gastaldo, Dan; Murray, Aaron; Ryba, Steven
Patent: US2013/224816 A1, 2013 ;
Location in patent: Paragraph 0287-0293 ;
反应条件
hydrogenchloride in ligroin; water; benzene
参考文献
A. H. Robins Company, Incorporated
Patent: US4950674 A1, 1990 ;
反应条件
hydrogen T=305°C; P=91809.2 Torr; 0.75 h; Sealed tube;
参考文献
CHEMTEX ITALIA, S.P.A.; Elliott, Guliz Arf; Gastaldo, Dan; Murray, Aaron; Ryba, Steven
Patent: US2013/224816 A1, 2013 ;
Location in patent: Paragraph 0287-0293 ;
反应条件
1,3-dimethyl-imidazolidin-2-one; sodium hexamethyldisilazane in tetrahydrofuran T=185°C; 12 h;
参考文献
Hwu, Jih Ru; Wong, Fung Fuh; Huang, Jiann-Jyh; Tsay, Shwu-Chen
Journal of Organic Chemistry, 1997 , vol. 62, # 12 p. 4097 - 4104
