3,6-二甲基-1,2-苯二酚合成路线 (共 25 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol
P=5171.5 Torr;
参考文献
Bell, Thomas W.; Lein, George M.; Nakamura, Hideo; Cram, Donald J.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4728 - 4734
反应条件
hydrogen; palladium on activated charcoal
参考文献
Fields,D.L. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2640 - 2647
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in chloroform
T=-25°C; 12 h;
参考文献
Pezzella, Alessandro; Lista, Liliana; Napolitano, Alessandra; D'Ischia, Marco
Tetrahedron Letters, 2005 , vol. 46, # 20 p. 3541 - 3544
反应条件
1: H3BO3; glycerol
2: amalgamated zinc; aqueous HCl
View Scheme
参考文献
Baker et al.
Journal of the Chemical Society, 1953 , p. 1615,1618
Journal of the Chemical Society, 1954 , p. 2042,2044
反应条件
hydrogenchloride in methanol
4 h; Heating;
参考文献
Sinhababu, Achintya K.; Borchardt, Ronald T.
Synthetic Communications, 1982 , vol. 12, # 12 p. 983 - 988
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Baines,M.W. et al.
J. Med. Chem., 1965 , vol. 8, p. 81 - 90
反应条件
1: LiAlH4
2: H2 / Pd-C / ethanol
View Scheme
参考文献
Baines,M.W. et al.
J. Med. Chem., 1965 , vol. 8, p. 81 - 90
反应条件
1: H2SO4
2: LiAlH4
3: H2 / Pd-C / ethanol
View Scheme
参考文献
Baines,M.W. et al.
J. Med. Chem., 1965 , vol. 8, p. 81 - 90
反应条件
tetreamethyl ammonium hydroxide; dihydrogen peroxide
参考文献
Baker et al.
Journal of the Chemical Society, 1953 , p. 1615,1618
Journal of the Chemical Society, 1954 , p. 2042,2044
反应条件
1: 94 percent / aq. HClO4, H2 / Pd/C / ethyl acetate / 1.5 h / 2585.7 Torr
2: 97 percent / aq. HCl / methanol / 4 h / Heating
View Scheme
参考文献
Sinhababu, Achintya K.; Borchardt, Ronald T.
Synthetic Communications, 1982 , vol. 12, # 12 p. 983 - 988