2-羟基-1,2-二(2-噻吩基)乙烷-1-酮合成路线 （共 9 条）
反应条件
1,12-bis((1-methylbenzimidazolium)-3-yl)dodecane dibromide; 1,8-diazabicyclo[5.4.0]undec-7-ene in water T=20°C; 1.5 h;
参考文献
Iwamoto, Ken-Ichi; Kimura, Hitomi; Oike, Masaaki; Sato, Masayuki
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 5 p. 912 - 915
反应条件
triethylamine; 5-(2-hydroxyethyl)-4-methyl-3-(phenylmethyl)thiazolium chloride in various solvent(s) T=80°C; Stetter reaction; 10 h;
参考文献
Anjaiah, Siddam; Chandrasekhar, Srivari; Gree, Rene
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 11 p. 1329 - 1334
反应条件
3-benzyl-5-(3-hydroxyethyl)-4-methylthiazol-3-ium bromide; triethylamine in ethanol 2 h; other aldehydes of heterocyclic aromatic compounds, var. catalysts and reaction time; Product distribution;
参考文献
Lee, Chang Kiu; Kim, Mi Soon; Gong, Jin Soon; Lee, In-Sook Han
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 1 p. 149 - 153
反应条件
oxygen; sodium hydride in tetrahydrofuran; mineral oil T=25°C; P=760.051 Torr; 0.75 h;
参考文献
Kang, Sunhae; Joo, Cheonik; Kim, Sun Min; Han, Hogyu; Yang, Jung Woon
Tetrahedron Letters, 2011 , vol. 52, # 4 p. 502 - 504
反应条件
air; tri-phenyl-antimony in dichloromethane T=20°C; 8 h;
参考文献
Yasuike, Shuji; Kishi, Yoshihito; Kawara, Shin-Ichiro; Kurita, Jyoji
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 4 p. 425 - 427
反应条件
sodium tetrahydroborate in ethanol; water T=0 - 20°C; 2 h;
参考文献
Lee, Chang Kiu; Kim, Mi Soon; Gong, Jin Soon; Lee, In-Sook Han
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 1 p. 149 - 153
反应条件
sulfuric acid T=20°C; 24 h;
参考文献
Morrison, Brian J.; Musgrave, Oliver C.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 17 p. 1944 - 1947
反应条件
diethylamine in N,N-dimethyl-formamide
24 h;
参考文献
Prousek, Josef; Jurasek, Adolf; Kovac, Jaroslav
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 5 p. 1581 - 1588
反应条件
air in tetrahydrofuran; ethyl acetate
T=20°C;
参考文献
Hu, Zhong-Yuan; Du, Ding; Tang, Wei-Fang; Lu, Tao
Asian Journal of Chemistry, 2012 , vol. 24, # 5 p. 2262 - 2264
