甲基 2-乙酰氨基-3,4,6-O-三乙酰基-2-脱氧-beta-D-吡喃葡萄糖苷合成路线 （共 48 条）
反应条件
3 A molecular sieve; TiF4 in acetonitrile 12 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Thiem, Joachim; Wiesner, Matthias
Carbohydrate Research, 1993 , vol. 249, # 1 p. 197 - 206
反应条件
trimethylsilyl trifluoromethanesulfonate in nitromethane glycosylation; 2 h; Heating; Title compound not separated from byproducts;
参考文献
Kadokawa, Jun-ichi; Nagaoka, Takeshi; Ebana, Jun; Tagaya, Hideyuki; Chiba, Koji
Carbohydrate Research, 2000 , vol. 327, # 3 p. 341 - 344
反应条件
methanol; sulfuric acid 1.) reflux, 2.) ether extraction, aqueous phase: 3.) pyridine, RT, 19 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nishizawa; Nishide; Kosela; Hayashi
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4462 - 4466
反应条件
trimethylsilyl trifluoromethanesulfonate 1.) CH2Cl2, 60 min, 2.) CH2Cl2, 30 min; Yield given. Multistep reaction;
参考文献
D'Ambra; Gray
Carbohydrate Research, 1994 , vol. 251, p. 115 - 125
参考文献
Cutler et al.
Journal of the Chemical Society, 1937 , p. 1979,1981
反应条件
1: 10 percent NH4OH-MeOH / Ambient temperature 2: 10 percent aq. H2SO4 / 1 h / 100 °C View Scheme
参考文献
Hirsch, S.; Kashman, Y.
Tetrahedron, 1989 , vol. 45, # 12 p. 3897 - 3906
反应条件
N(Et)4ClO4 in methanol electrolysis, Au anode, 0.06 A/cm2;
参考文献
Imagawa, Takeshi; Nakashima, Yasushi; Kawanisi, Mituyosi
Chemistry Letters, 1980 , p. 1609 - 1612
反应条件
Biorad AGMP(OH-) resin in methanol
参考文献
RajanBabu; Ayers, Timothy A.; Halliday, Gary A.; You, Kimberly K.; Calabrese, Joseph C.
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 6012 - 6025
