反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
1.2: 13 h / 20 - 50 °C / Inert atmosphere
2.1: 5 Pd(II)/C(eggshell); hydrogen; acetic acid / ethanol / 12 h / 3102.97 Torr
3.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
4.1: trichlorophosphate / dichloromethane / 3 h / 120 °C / Inert atmosphere
View Scheme
参考文献
Gao, Kai; Yu, Chang-Bin; Li, Wei; Zhou, Yong-Gui; Zhang, Xumu
Chemical Communications, 2011 , vol. 47, # 27 p. 7845 - 7847