N-[2-(苯氧基)苯基]甲酰胺合成路线 (共 6 条)
反应条件
triethylamine; trichloromethyl chloroformate in dichloromethane 0 deg C, 30 min then r.t.;
参考文献
Leardini, Rino; McNab, Hamish; Nanni, Daniele
Tetrahedron, 1995 , vol. 51, # 44 p. 12143 - 12158
反应条件
in toluene
8 h; Heating;
参考文献
Okubo, Taketoshi; Yoshikawa, Ryoko; Chaki, Shigeyuki; Okuyama, Shigeru; Nakazato, Atsuro
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 2 p. 423 - 438
反应条件
(i) Raney-Ni, H2, (ii) (formylation); Multistep reaction;
参考文献
Higginbottom,R.; Suschitzky,H.
Journal of the Chemical Society, 1962 , p. 2367 - 2370
参考文献
v.Braun; Weissbach
Chemische Berichte, 1932 , vol. 65, p. 1574,1579
反应条件
polyphosphiric acid; trichlorophosphate
T=120 - 130°C; Cyclization; 2 h;
参考文献
Noskov; Kalinina; Noskova; Kruglyak; Strukov; Bezrukov; Kurochkin
Pharmaceutical Chemistry Journal, 1997 , vol. 31, # 8 p. 431 - 434
反应条件
triethylamine; trichloromethyl chloroformate in dichloromethane
0 deg C, 30 min then r.t.;
参考文献
Leardini, Rino; McNab, Hamish; Nanni, Daniele
Tetrahedron, 1995 , vol. 51, # 44 p. 12143 - 12158