1-(苄基磺酰基)-4-硝基苯合成路线 (共 45 条)
反应条件
palladium diacetate; potassium carbonate; thiourea; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water T=20°C; 2 h; Inert atmosphere;
参考文献
Wang, Liang; Zhou, Wei-You; Chen, Sheng-Chun; He, Ming-Yang; Chen, Qun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 839 - 845
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide 0.25 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
tetra(n-butyl)ammonium hydroxide; sodium hydroxide; palladium dichloride in water T=70°C; 0.1 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Rostami, Abed
Applied Organometallic Chemistry, 2013 , vol. 27, # 9 p. 501 - 506
反应条件
1: benzyl chloride With [2,2']bipyridinyl; CuSO4‵5H2O; sodium thiosulfate * H2O in methanol; water T=80°C; 2 h; Schlenk technique; 2: 4-nitro-aniline With tert.-butylnitrite in methanol; water T=0 - 80°C; 4.66667 h; Schlenk technique;
参考文献
Li, Yiming; Pu, Jiahua; Jiang, Xuefeng
Organic Letters, 2014 , vol. 16, # 10 p. 2692 - 2695
反应条件
tetra-(n-butyl)ammonium iodide; potassium hydrogencarbonate; palladium diacetate; triphenylphosphine in 1,4-dioxane T=100°C; sulfenylation; 6 h;
参考文献
Harayama, Hiroto; Nagahama, Takayuki; Kozera, Toyohiro; Kimura, Masanari; Fugami, Keigo; Tanaka, Shuji; Tamaru, Yoshinao
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 2 p. 445 - 456
反应条件
cesium fluoride in acetonitrile T=82°C;
参考文献
Shah, Syed Tasadaque Ali; Khan, Khalid Mohammed; Martinez Heinrich, Angelica; Voelter, Wolfgang
Tetrahedron Letters, 2002 , vol. 43, # 46 p. 8281 - 8283
Title/Abstract Full Text View citing articles Show Details
Shah, Syed T. A.; Khan, Khalid M.; Hussain, Hidayat; Hayat, Safdar; Voelter, Wolfgang
Monatshefte fur Chemie, 2005 , vol. 136, # 9 p. 1583 - 1589
反应条件
palladium diacetate; potassium carbonate; thiourea; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in water T=20°C; 12 h; Inert atmosphere;
参考文献
Wang, Liang; Zhou, Wei-You; Chen, Sheng-Chun; He, Ming-Yang; Chen, Qun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 839 - 845
反应条件
tetra(n-butyl)ammonium hydroxide; sodium hydroxide; palladium dichloride in water T=70°C; 1 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Rostami, Abed
Applied Organometallic Chemistry, 2013 , vol. 27, # 9 p. 501 - 506
反应条件
tetra(n-butyl)ammonium hydroxide; sodium hydroxide; palladium dichloride in water T=70°C; 4.5 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Rostami, Abed
Applied Organometallic Chemistry, 2013 , vol. 27, # 9 p. 501 - 506
反应条件
copper(l) iodide; potassium carbonate; thiourea in water T=80°C; 12 h; Inert atmosphere;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Gholinejad, Mohammad
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 1 p. 119 - 124