(1E)-3-甲基-1-硝基-1-丁烯合成路线 （共 12 条）
反应条件
sodium hydroxide in methanol T=0°C; 1 h;
参考文献
Kumaran; Kulkarni
Synthesis, 1995 , # 12 p. 1545 - 1548
反应条件
H-Y zeolite in toluene 8 h; Heating;
参考文献
Anbazhagan; Kumaran; Sasidharan
Journal of Chemical Research - Part S, 1997 , # 9 p. 336 - 337
反应条件
dicyclohexyl-carbodiimide; copper(l) chloride in diethyl ether Dehydration; 12 h; Title compound not separated from byproducts;
参考文献
Lucet, Denis; Sabelle, Stephane; Kostelitz, Olivier; Le Gall, Thierry; Mioskowski, Charles
European Journal of Organic Chemistry, 1999 , # 10 p. 2583 - 2591
反应条件
sodium carbonate; benzene
参考文献
Sanno et al.
Yakugaku Zasshi, 1955 , vol. 75, p. 1461,1465
Chem.Abstr., 1956 , p. 10708
Full Text Show Details
Drake; Ross
Journal of Organic Chemistry, 1958 , vol. 23, p. 717,720
反应条件
methanesulfonyl chloride; triethylamine Yield given;
参考文献
Munk; Lai; Burke; Arasasingham; Kharlamb; Manlapaz; Padillo; Wijono; Hasson; Wheeler; Garst
Journal of Medicinal Chemistry, 1996 , vol. 39, # 6 p. 1193 - 1195
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tert-butyl alcohol ΔGchem; Equilibrium constantThermodynamic data;
参考文献
Hine, Jack; Linden, Shwn-Meei
Journal of Organic Chemistry, 1983 , vol. 48, # 4 p. 584 - 587
参考文献
Sanno et al.
Yakugaku Zasshi, 1955 , vol. 75, p. 1461,1465
Chem.Abstr., 1956 , p. 10708
Full Text Show Details
Drake; Ross
Journal of Organic Chemistry, 1958 , vol. 23, p. 717,720
反应条件
1: 92 percent / CH2Cl2 / 20 h / Ambient temperature 2: 1.) O3, 2.) Me2S / 1.) CH2Cl2, -78 deg C, 2.) CH2Cl2, from -78 deg C to RT View Scheme
参考文献
Lassaletta, Jose-Maria; Fernandez, Rosario; Gasch, Consolacion; Vazquez, Juan
Tetrahedron, 1996 , vol. 52, # 27 p. 9143 - 9160
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tert-butyl alcohol ΔGchem; Equilibrium constantThermodynamic data;
参考文献
Hine, Jack; Linden, Shwn-Meei
Journal of Organic Chemistry, 1983 , vol. 48, # 4 p. 584 - 587
反应条件
1.1: potassium tert-butoxide; 18-crown-6 / tetrahydrofuran / 1 h / 0 °C 1.2: 87 percent / tetrahydrofuran / 0.25 h / -78 °C 2.1: 51 percent / sodium nitrite; acetic acid / dimethylsulfoxide / 28 h / 40 °C 3.1: 62 percent / lithium; NH3 / tetrahydrofuran; 2-methyl-propan-2-ol / 0.5 h / -78 °C View Scheme
参考文献
Lucet, Denis; Sabelle, Stephane; Kostelitz, Olivier; Le Gall, Thierry; Mioskowski, Charles
European Journal of Organic Chemistry, 1999 , # 10 p. 2583 - 2591
