3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛烷磺酰氯合成路线 （共 2 条）
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27619-89-23,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛烷磺酰氯
反应条件
water; chlorine in acetic acid T=45°C; 10 h;
参考文献
Taylor, Charles Kenneth; Michalczyk, Michael Joseph; Acosta, Erick Jose
Patent: US2009/42996 A1, 2009 ;
Location in patent: Page/Page column 6-7 ;
27619-97-23,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛磺酸
→
27619-89-23,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛烷磺酰氯
反应条件
phosphorus pentachloride; trichlorophosphate T=20 - 60°C; 78 h;
参考文献
BAYER SCHERING PHARMA AKTIENGESELLSCHAFT; SRINIVASAN, Ananth; BERNDT, Mathias; GRAHAM, Keith; FRIEBE, Matthias; SCHMITT-WILLICH, Heribert
Patent: WO2010/409 A2, 2010 ;
Location in patent: Page/Page column 21-22 ;
