3-甲基-2-环戊烯-1-酮合成路线 （共 109 条）
反应条件
boron trifluoride diethyl etherate in dichloromethane T=0°C; 2 h;
参考文献
Smith,A.B.; Toder,B.H.; Branca,S.J.
Journal of the American Chemical Society, 1981 , vol. 103, p. 1996
反应条件
cesium hydroxide in water
参考文献
BASF Aktiengesellschaft
Patent: US5077438 A1, 1991 ;
反应条件
sodium hydroxide in water
参考文献
Ethyl Corporation
Patent: US5276199 A1, 1994 ;
反应条件
Amberlyst 15; sodium iodide in acetone T=20°C; deoxygenation; 3 h;
参考文献
Righi, Giuliana; Bovicelli, Paolo; Sperandio, Anna
Tetrahedron, 2000 , vol. 56, # 12 p. 1733 - 1737
反应条件
aluminium trichloride in dichloromethane 10 h; Ambient temperature;
参考文献
Kishi; Mikami; Nakai
Tetrahedron, 1991 , vol. 47, # 38 p. 8111 - 8118
反应条件
1: With tert.-butylhydroperoxide; 3 A molecular sieve in decane; ethyl acetate T=20°C; 0.5 h; 2: With oxygen; manganese triacetate in decane; ethyl acetate T=20°C; 48 h;
参考文献
Shing, Tony K. M.; Yeung, Ying-Yeung; Su, Pak L.
Organic Letters, 2006 , vol. 8, # 14 p. 3149 - 3151
反应条件
carbon dioxide; oxygen; 1-hydroxy-pyrrolidine-2,5-dione; anhydrous cobalt diacetate T=100°C; P=44734.5 Torr; 1 h; Product distribution / selectivity;
参考文献
University of Kansas
Patent: US2008/139841 A1, 2008 ;
Location in patent: Page/Page column 8 ;
反应条件
potassium carbonate in tetrahydrofuran 8 h; Heating;
参考文献
Hendrickson, James B.; Palumbo, Paul S.
Journal of Organic Chemistry, 1985 , vol. 50, # 12 p. 2110 - 2112
反应条件
pyridine; ruthenium trichloride; ruthenium(IV) chloride in water T=130°C; P=760000 Torr;
参考文献
Kealy,T.J.; Benson,R.E.
Journal of Organic Chemistry, 1961 , vol. 26, p. 3126 - 3130
反应条件
hydrogenchloride; acetic acid T=100°C; 4 h;
参考文献
Ho, Tse-Lok; Lui, Shing-Hou
Synthetic Communications, 1983 , vol. 13, # 8 p. 685 - 690
