1,7,7-三甲基-2-亚甲基-降冰片烷合成路线 （共 8 条）
反应条件
titanium tetrachloride; magnesium in tetrahydrofuran T=0 - 20°C; 1 h;
参考文献
Yan, Tu-Hsin; Tsai, Chia-Chung; Chien, Ching-Ting; Cho, Chia-Ching; Huang, Pei-Chen
Organic Letters, 2004 , vol. 6, # 26 p. 4961 - 4963
反应条件
titanium(III) chloride in tetrahydrofuran THF, reflux, 5 h;
参考文献
Welch, Steven C.; Loh, Jiann-Ping
Journal of Organic Chemistry, 1981 , vol. 46, # 20 p. 4072 - 4074
反应条件
in benzene T=90 - 100°C; 2 h;
参考文献
Fitjer, Lutz; Quabeck, Ulrike
Synthetic Communications, 1985 , vol. 15, # 10 p. 855 - 864
反应条件
in pentane 0.0333333 h; Ambient temperature;
参考文献
Dormond, Alain; Bouadili, Abdelaziz El; Moise, Claude
Journal of Organic Chemistry, 1987 , vol. 52, # 4 p. 688 - 689
反应条件
titanium tetrachloride; zinc in tetrahydrofuran; dichloromethane T=25°C; 40 h;
参考文献
Takai, Kazuhiko; Hotta, Yuji; Oshima, Koichiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 6 p. 1698 - 1702
反应条件
pyridine; thionyl chloride Dehydration; Product distribution; Further Variations:Reagents;
参考文献
Schumann, Russell; Pendleton, Phillip
Water Research, 1997 , vol. 31, # 5 p. 1243 - 1246
反应条件
in diethyl ether Heating;
参考文献
Spear, Robert J.; Sternhell, Sever
Australian Journal of Chemistry, 1985 , vol. 38, # 6 p. 889 - 897
参考文献
Ruzicka
Helvetica Chimica Acta, 1918 , vol. 1, p. 116
