反应条件
1: <1,3-bis(diphenylphosphino)propane>nickel dichloride ((dppp)NiCl2) / benzene / 20 h / 70 °C 2: 1.) methyllithium / 1.) ether, 0 deg C, 30 min, 2.) 0 deg C 3: 1.) cuprous cyanide, lithium chloride / 1.) THF, ether, -10 deg C, 2.) a) -10 deg C, 1 h, b) 0 deg C, 2 h, c) RT, 1 h View Scheme
参考文献
Wenkert, Ernest; Ferreira, Vitor F.; Michelotti, Enrique L.; Tingoli, Marco
Journal of Organic Chemistry, 1985 , vol. 50, # 5 p. 719 - 721
