顺-5-降冰片烯-外型-2,3-二甲酸酐合成路线 （共 22 条）
反应条件
1: hepta-1,6-dien-3-yl 2,2,2-trichloroacetate With copper(l) chloride; Grubb's 2nd generation catalyst in chloroform-d1 T=20°C; 2 h; 2: maleic anhydride in chloroform-d1 Diels-Alder reaction; 3 h; Heating;
参考文献
Edlin, Chris D.; Faulkner, James; Quayle, Peter
Tetrahedron Letters, 2006 , vol. 47, # 7 p. 1145 - 1151
反应条件
sodium hydroxide in water T=70°C; 0.166667 h; Product distribution / selectivity;
参考文献
Hitachi Chemical Co., Ltd.
Patent: EP1669342 A1, 2006 ;
Location in patent: Page/Page column 21 ;
参考文献
ISP INVESTMENTS INC.; MUSA, Osama, M.; EZAT, Khosravi
Patent: WO2010/101882 A1, 2010 ;
Location in patent: Page/Page column 15 ;
反应条件
[C6mim][BF4] T=20°C; Diels-Alder reaction; 0.0833333 h;
参考文献
Silvero, Guadalupe; Arevalo, Maria Jose; Bravo, Jose Luis; Avalos, Martin; Jimenez, Jose Luis; Lopez, Ignacio
Tetrahedron, 2005 , vol. 61, # 30 p. 7105 - 7111
反应条件
1.1: 95 percent / Et3N / diethyl ether / 0 °C 2.1: CuCl / (PCy3)Cl2Ru=CHPh(diMsIm) / CDCl3 / 2 h / 20 °C 2.2: 92 percent / CDCl3 / 3 h / Heating View Scheme
参考文献
Edlin, Chris D.; Faulkner, James; Quayle, Peter
Tetrahedron Letters, 2006 , vol. 47, # 7 p. 1145 - 1151
反应条件
2-acetyloxy-1-propene; Montmorillonite KSF 0.0666667 h; Irradiation;
参考文献
Villemin; Labiad; Loupy
Synthetic Communications, 1993 , vol. 23, # 4 p. 419 - 424
反应条件
T=206°C; Diels-Alder reaction; 0.366667 h; Neat (no solvent);
参考文献
Huertas, David; Florscher, Melinda; Dragojlovic, Veljko
Green Chemistry, 2009 , vol. 11, # 1 p. 91 - 95
反应条件
indium(III) chloride in water 4 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
De La Torre, Maria Fe; Caballero, M. Cruz; Whiting, Andrew
Tetrahedron, 1999 , vol. 55, # 28 p. 8547 - 8554
反应条件
T=200°C; P=100 Torr;
参考文献
Craig
Journal of the American Chemical Society, 1951 , vol. 73, p. 4889,4891
参考文献
Pirsch
Monatshefte fuer Chemie, 1955 , vol. 86, p. 216,220
Microchimica Acta, 1956 , p. 992,1000
Full Text Show Details
Alder; Stein
Justus Liebigs Annalen der Chemie, 1933 , vol. 504, p. 216,232, 252
Justus Liebigs Annalen der Chemie, 1935 , vol. 515, p. 185,187
