反应条件
AgClO4 in water; 1,2-dichloro-ethane byproducts: AgCl; to soln. (TMNA)PdCl(DMPP) in 1,2-dichloroethane was added soln. AlClO4 in water and mixt. was stirred for 30 min, mixt. was filtered, organic layer was dried over MgSO4, ADPP was added, react. mixt. was stirred under N2 for 6 days at 75°C; solvent was removed under reduced pressure, residue was chromed. on silica with CH2Cl2/ethylacetate (4:1); elem. anal.;
参考文献
Organometallics, , vol. 19, p. 91 - 104
