1,3-苯并间二氧杂环戊烯合成路线 （共 145 条）
反应条件
potassium carbonate in methanol; pinacolate ester
参考文献
Commonwealth Scientific and Industrial Research Organization
Patent: US6448433 B1, 2002 ;
反应条件
potassium carbonate in N-methyl-acetamide; benzene
参考文献
L'Oreal
Patent: US4865617 A1, 1989 ;
反应条件
1.54H2O*Cl2Ni; ICy*HBF4 in tetrahydrofuran T=-10°C; Kumada coupling reaction; 1.5 h; Inert atmosphere;
参考文献
Joshi-Pangu, Amruta; Wang, Chao-Yuan; Biscoe, Mark R.
Journal of the American Chemical Society, 2011 , vol. 133, # 22 p. 8478 - 8481
反应条件
bis(acetylacetonate)nickel(II); manganese; 2,9-dimethyl-1,10-phenanthroline in N,N-dimethyl acetamide T=20°C; 1 h;
参考文献
Shrestha, Ruja; Dorn, Stephanie C. M.; Weix, Daniel J.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 751 - 762
反应条件
lt;Pgt;-(CH2)3-+PBu3 in water T=110°C; 2 h;
参考文献
Chiles, Margaret Shea; Jackson, Donald D.; Reeves, Perry C.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2915 - 2918
反应条件
sodium t-butanolate; palladium diacetate; tri-tert-butyl phosphine in o-xylene T=120°C; Yield given;
参考文献
Nishiyama, Masakazu; Yamamoto, Toshihide; Koie, Yasuyuki
Tetrahedron Letters, 1998 , vol. 39, # 7 p. 617 - 620
反应条件
1: With (HOCH2)2CMeCH2O-polymer in tetrahydrofuran Cyclization; 2: With Ag(NH3)NO3 in tetrahydrofuran Protodeboronation; 8 h; Heating; Further stages.;
参考文献
Pourbaix, Christelle; Carreaux, Francois; Carboni, Bertrand; Deleuze, Herve
Chemical Communications, 2000 , # 14 p. 1275 - 1276
参考文献
Warner-Lambert Company
Patent: US5482960 A1, 1996 ;
US 5482960 A
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; 4-bromooctafluorobutanetriethoxysilane in N,N-dimethyl-formamide T=20°C; 0.5 h; Inert atmosphere;
参考文献
Tang, Zhi Yong; Zhang, Yuan; Wang, Tao; Wang, Wei
Synlett, 2010 , # 5 art. no. W16209ST, p. 804 - 808
反应条件
palladium diacetate; tri-tert-butyl phosphine in xylene T=120°C; Substitution; Suzuki coupling; 6 h;
参考文献
Watanabe, Makoto; Nishiyama, Masakazu; Koie, Yasuyuki
Tetrahedron Letters, 1999 , vol. 40, # 50 p. 8837 - 8840
