1,3-苯并间二氧杂环戊烯合成路线 （共 145 条）
反应条件
potassium phosphate in N,N-dimethyl-formamide; cyclohexanol T=110°C; 12 h;
参考文献
Min, Hongkeun; Lee, Sunyoung; Park, Minhan; Hwang, Jinil; Jung, Hyun Min; Lee, Sunwoo
Journal of Organometallic Chemistry, 2014 , vol. 755, p. 7 - 11
反应条件
sodium hydroxide in dimethyl sulfoxide T=80°C; Reflux;
参考文献
GRUeNENTHAL GMBH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; SCHIENE, Klaus; DE VRY, Jean; DAMANN, Nils; FRORMANN, Sven; LESCH, Bernhard; LEE, Jeewoo; KIM, Yong-Soo; KIM, Myeong-Seop
Patent: WO2010/127855 A1, 2010 ;
Location in patent: Page/Page column 114 ;
反应条件
1: With ethidium Bromide; magnesium; iron(II) chloride; magnesium chloride in tetrahydrofuran T=22 - 52°C; 23 h; 2: With water in tetrahydrofuran
参考文献
Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Green Chemistry, 2009 , vol. 11, # 7 p. 942 - 945
反应条件
potassium carbonate; palladium monocarbide in methanol
参考文献
Commonwealth Scientific and Industrial Research Organization
Patent: US6448433 B1, 2002 ;
反应条件
N-ethyl-N,N-diisopropylamine; biphenyl-2-yl-di-tert-butyl-phosphane; bis(dibenzylideneacetone)-palladium(0) in 1-methyl-pyrrolidin-2-one T=60°C; 12 h;
参考文献
Manoso; DeShong
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7449 - 7455
反应条件
triethylamine in 2,2,2-trifluoroethanol 7 h; Photolysis;
参考文献
Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2007 , vol. 46, # 34 p. 6495 - 6498
反应条件
sodium hydroxide in dichloromethane; water; dimethyl sulfoxide
参考文献
Eli Lilly and Company
Patent: US4082774 A1, 1978 ;
反应条件
caesium carbonate in N,N-dimethyl-formamide T=20 - 110°C;
参考文献
Cabiddu, Maria Grazia; Cadoni, Enzo; De Montis, Stefania; Fattuoni, Claudia; Melis, Stefana; Usai, Michele
Tetrahedron, 2003 , vol. 59, # 24 p. 4383 - 4387
反应条件
tetraethylammonium p-toluenesulfonate; triphenylphosphine; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide Pt anode/Pt cathode; electrolysis with 2.5 mA/cm2;
参考文献
Torii, Sigeru; Tanaka, Hideo; Hamatani, Takeshi; Morisaki, Kazuo; Jutand, Anny; et al.
Chemistry Letters, 1986 , p. 169 - 172
反应条件
TS-2 in 1,4-dioxane T=330°C; 5 h; Gas phase; Product distribution / selectivity;
参考文献
RHODIA CHIMIE
Patent: US2008/21228 A1, 2008 ;
Location in patent: Page/Page column 5 ;
