苯并[d]噁唑-2-羧酸甲酯合成路线 （共 12 条）
反应条件
1: 1,3-benzoxazole; carbon dioxide With caesium carbonate in N,N-dimethyl-formamide T=125°C; P=1064.07 Torr; 16 h; 2: methyl iodide in N,N-dimethyl-formamide Heating;
参考文献
Boogaerts, Ine I. F.; Nolan, Steven P.
Journal of the American Chemical Society, 2010 , vol. 132, # 26 p. 8858 - 8859
反应条件
triethylamine 3 h; Reflux;
参考文献
Vodela, Sunil; Mekala, Raghu Vardhan Reddy; Danda, Ravinder Reddy; Kodhati, Venkateshwarlu
Chinese Chemical Letters, 2013 , vol. 24, # 7 p. 625 - 628
参考文献
Musser, J. H.; Hudec, T. T.; Bailey, K.
Synthetic Communications, 1984 , vol. 14, # 10 p. 947 - 954
反应条件
1: C27H37ClCuN3; potassium tert-butylate / tetrahydrofuran / 8 h / 80 °C / 760.05 Torr / Inert atmosphere; sealed tube 2: N,N-dimethyl-formamide / 1 h / 80 °C / Inert atmosphere; sealed tube View Scheme
参考文献
Nolan, Steven P.; Cazin, Catherine
Patent: US2013/85276 A1, 2013 ;
反应条件
in N,N-dimethyl-formamide T=80°C; 1 h; Inert atmospheresealed tube;
参考文献
Nolan, Steven P.; Cazin, Catherine
Patent: US2013/85276 A1, 2013 ;
Location in patent: Paragraph 0102 ;
反应条件
1: thionyl chloride / ethanol / 4 h / 20 °C 2: triethylamine / 3 h / |Reflux View Scheme
参考文献
Vodela, Sunil; Mekala, Raghu Vardhan Reddy; Danda, Ravinder Reddy; Kodhati, Venkateshwarlu
Chinese Chemical Letters, 2013 , vol. 24, # 7 p. 625 - 628
反应条件
1: dimethylsulfoxide; propan-2-ol 2: K2CO3 3: aq. HCl View Scheme
参考文献
Moeller,H.
Justus Liebigs Annalen der Chemie, 1971 , vol. 749, p. 1 - 11
反应条件
1: K2CO3 2: aq. HCl View Scheme
参考文献
Moeller,H.
Justus Liebigs Annalen der Chemie, 1971 , vol. 749, p. 1 - 11
参考文献
Dickore,K. et al.
Justus Liebigs Annalen der Chemie, 1970 , vol. 733, p. 70 - 87
参考文献
Pfizer Inc.
Patent: US4826833 A1, 1989 ;
US 4826833 A
