反应条件
1: 70 percent / NaN(SiMe3)2 2: 100 percent / H+ / tetrahydrofuran 3: 81 percent / NaBH4 / aq. ethanol / 1.) 0 deg C, 5 min, 2.) room temperature, 5 min 4: 91 percent / Ph3PBr2 / acetonitrile 5: 89 percent / acetonitrile / 24 h / Heating 6: 60 percent / NaN(SiMe3)2 / tetrahydrofuran / 1.) room temperature, 1 h, 2.) -90 deg C View Scheme
参考文献
Sandri; Viala
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6627 - 6630
