1: With hydrogenchloride; thionyl chloride in 1,4-dioxane T=20 - 40°C; 20 h; 2: in water T=0 - 20°C; 0.166667 h; 3: With lithium hydroxide in water T=0 - 10°C; pH=5.5;
参考文献
Kaneka Corporation
Patent: US6372941 B1, 2002 ;
Location in patent: Example 4 ;
Axelsson, B. Svante; O'Toole, Kevin J.; Spencer, Philip A.; Young, Douglas W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 7 p. 807 - 816