1-氯-3,3,3-三氟丙烯合成路线 (共 42 条)
反应条件
ammonium formate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=-30 - 100°C; 24 h;
参考文献
Honeywell International Inc.
Patent: US6958424 B1, 2005 ;
Location in patent: Page/Page column 9 ;
反应条件
1: With hydrogen fluoride; titanium tetrachloride T=20 - 120°C; P=18617.8 Torr; 1.16667 h; 2: With potassium hydroxide in water
参考文献
Honeywell International Business Machines
Patent: US6844475 B1, 2005 ;
Location in patent: Page column 3 ;
反应条件
hydrogen fluoride; chlorine; antimony(V) pentachloride T=80 - 95°C; P=8517.48 - 10069 Torr;
参考文献
Honeywell International, Inc.
Patent: US2005/90698 A1, 2005 ;
Location in patent: Page/Page column 5 ;
反应条件
1: With hydrogen fluoride; titanium tetrachloride T=90°C; P=10343.2 Torr; 2: With potassium hydroxide in water T=30°C;
参考文献
Central Glass Company, Limited
Patent: EP2341040 A1, 2011 ;
Location in patent: Page/Page column 14-15 ;
反应条件
hydrogen fluoride; SbF5 T=120 - 121°C; P=9551.8 - 29721.1 Torr; 3.5 h; Product distribution / selectivity;
参考文献
HONEYWELL INTERNATIONAL INC.; Nair, Haridasan K.; Singh, Rajiv Ratna; Poss, Andrew Joseph; Nalewajek, David
Patent: US2013/211156 A1, 2013 ;
Location in patent: Paragraph 0033; 0034 ;
反应条件
fluorinated Cr2O3 T=225°C; P=760.051 Torr;
参考文献
Wang, Haiyou; Tung, Hsueh Sung
Patent: US2012/271069 A1, 2012 ;
Location in patent: Page/Page column 3-4 ;
反应条件
hydrogen fluoride; SbF5 T=120 - 121°C; P=9551.8 - 29721.1 Torr; 3.5 h; Product distribution / selectivity;
参考文献
Honeywell International Inc.
Patent: US2007/118003 A1, 2007 ;
Location in patent: Page/Page column 4-5 ;
反应条件
hydrogen fluoride; Catalyst M-Chromium oxide T=300°C;
参考文献
Honeywell International, Inc.
Patent: US2005/90698 A1, 2005 ;
Location in patent: Page/Page column 5 ;
反应条件
chlorine; activated carbon catalyst T=250°C; P=760.051 Torr; Inert atmosphere; Product distribution / selectivity;
参考文献
INEOS FLUOR HOLDINGS LIMITED
Patent: WO2009/125200 A2, 2009 ;
Location in patent: Page/Page column 33 ;
反应条件
chlorine; carbon T=200°C; P=760.051 Torr; Product distribution / selectivity;
参考文献
INEOS FLUOR HOLDINGS LIMITED
Patent: WO2009/125200 A2, 2009 ;
Location in patent: Page/Page column 33 ;