3-(羟基甲基)-2,2,5,5-四甲基-1-吡咯烷醇合成路线 （共 5 条）
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in toluene
参考文献
Hideg, K.; Hankovszky, H. O.; Lex, L.; Kulcsar, Gy.
Synthesis, 1980 , # 11 p. 911 - 914
反应条件
1: 50 percent / Dicyclohexylcarbodiimide / ethyl acetate / 3 h / Ambient temperature 2: 47 percent / NaBH4 / ethanol / 6 h / Ambient temperature View Scheme
参考文献
Hideg, K.; Hankovszky, H. O.; Lex, L.; Kulcsar, Gy.
Synthesis, 1980 , # 11 p. 911 - 914
反应条件
sodium tetrahydroborate in ethanol 6 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hideg, K.; Hankovszky, H. O.; Lex, L.; Kulcsar, Gy.
Synthesis, 1980 , # 11 p. 911 - 914
反应条件
1: 95 percent / pyridine / 0 °C 2: 81 percent / NaN3 / H2O; dimethylformamide / 4 h / Heating 3: 87 percent / diethyl ether / Heating 4: 65 percent / PPh3 / 1 h / Heating View Scheme
参考文献
Hankovszky, H. O.; Hideg, K.; Lex, L.
Synthesis, 1981 , # 2 p. 147 - 149
反应条件
1: 95 percent / pyridine / 0 °C 2: 81 percent / NaN3 / H2O; dimethylformamide / 4 h / Heating 3: 87 percent / diethyl ether / Heating 4: 76 percent / aq. ethanol / 10 h / Heating View Scheme
参考文献
Hankovszky, H. O.; Hideg, K.; Lex, L.
Synthesis, 1981 , # 2 p. 147 - 149
