1-二(2,3,4,5,6-五氟苯基)磷酰-2,3,4,5,6-五氟苯合成路线 （共 12 条）
反应条件
potassium dichromate in sulfuric acid; acetic acid 6h heating under reflux;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.4, page 31 - 40
反应条件
in further solvent(s) solvent: Cl2CFCF2Cl; sealed tube, -70°C for 1 d, shaking at room temp. for 20 min, left standing for another d; recrystn. from petroleum ether;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.3, page 87 - 96
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.4, page 31 - 40
反应条件
water in neat (no solvent) hydrolysis;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.4, page 31 - 40
反应条件
water in acetonitrile T=20°C; 216 h;
参考文献
Frohn, Hermann-Josef; Wenda, Andre; Floerke, Ulrich
Tetrahedron, 2010 , vol. 66, # 31 p. 5762 - 5767
反应条件
in perchloric acid; acetonitrile Kinetics; 25°C;
参考文献
Abu-Omar; Espenson
Journal of the American Chemical Society, 1995 , vol. 117, # 1 p. 272 - 280
反应条件
potassium dichromate in sulfuric acid; water; acetic acid refluxing;
参考文献
Gmelin Handbook: F: PerFHalOrg.3, 1.12, page 137 - 160
反应条件
in further solvent(s) in Cl2CFCF2Cl, sealed ampule at -70°C for one day, shaking at room temp. for 20 min;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.11.1, page 149 - 158
反应条件
water; epoxysulfonyl fluoride dissolving (C6F5)3P in a SbF5-HSO3F mixt. (1:1); addn. of H2O;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.3, page 87 - 96
反应条件
C18F13H; C24F17H in diethyl ether; hexane 6 h at 25°C in ether/hexane 1:1;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.3, page 87 - 96
