in toluene Ce(O-i-Pr)4 is dissolved in toluene, soln. of n-Bu3SnCp is added, mixt. is heated at 65°C for 24 h (N2); mixt. is cooled to room temp., filtn., volatile components are removed under high vac., recrystn. at -78°C (pentane) or sublimation at 70°C (10E-5 Torr); elem. anal.;
参考文献
Gulino, Antonio; Casarin, Maurizio; Conticello, Vincent P.; Gaudiello, John G.; Mauermann, Heiko; et al.
Organometallics, 1988 , vol. 7, p. 2360 - 2364
Sakai et al.
Journal of the Chemical Society, Chemical Communications, 1975 , p. 265
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Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.4, page 61 - 63
