2,2',7,7'-四溴-9,9-联亚芴基合成路线 (共 10 条)
反应条件
anhydrous iron chloride; bromine in chloroform T=0°C; Reflux;
参考文献
UNIVERSITA DEGLI STUDI DI ROMA LA SAPIENZA; MATTIELLO, Leonardo; BAGALA' RAMPAZO, Liliana
Patent: WO2010/38251 A1, 2010 ;
Location in patent: Page/Page column 12-13 ;
反应条件
W(CO)6 in chlorobenzene Heating;
参考文献
Yeung, Lam Lung; Yip, Yu Chi; Luh, Tien-Yau
Journal of the Chemical Society, Chemical Communications, 1987 , # 13 p. 981 - 983
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile T=60°C; 2 h; Inert atmosphereDarkness;
参考文献
Brunetti; Gong; Tong; Heeger; Wudl, Fred
Angewandte Chemie - International Edition, 2010 , vol. 49, # 3 p. 532 - 536
反应条件
nitromethane; triethylamine T=100°C;
参考文献
Pinck; Hilbert
Journal of the American Chemical Society, 1946 , vol. 68, p. 2014,2016
反应条件
pyridine; potassium hydroxide
参考文献
Suzuki
Nippon Kagaku Zasshi, 1951 , vol. 72, p. 825,826
Chem.Abstr., 1953 , p. 7469
参考文献
Schmidt,J.; Wagner
Justus Liebigs Annalen der Chemie, 1912 , vol. 387, p. 155
参考文献
Schoenberg,A. et al.
Chemische Berichte, 1962 , vol. 95, p. 2144 - 2154
反应条件
1: PCl5 / 220 °C 2: copper powder; benzene View Scheme
参考文献
Schmidt,J.; Wagner
Justus Liebigs Annalen der Chemie, 1912 , vol. 387, p. 155
参考文献
Suzuki
Nippon Kagaku Zasshi, 1951 , vol. 72, p. 825,826
Chem.Abstr., 1953 , p. 7469
参考文献
Pinck; Hilbert
Journal of the American Chemical Society, 1946 , vol. 68, p. 2014,2016