4-(2-氯乙基)-1,2-二甲氧基苯合成路线 （共 15 条）
反应条件
thionyl chloride in chloroform 4 h; Heating / reflux;
参考文献
M'S SCIENCE CORPORATION
Patent: WO2008/96189 A2, 2008 ;
Location in patent: Page/Page column 27-28 ;
反应条件
1: (i) LiAlH4, Et2O, (ii) aq. H2SO4 2: SOCl2, PhNMe2 / CHCl3 View Scheme
参考文献
Campaigne,E.; Heaton,B.G.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2372 - 2378
反应条件
1: NaNO2; aqueous acetic acid 2: tetrachloromethane; PCl5 View Scheme
参考文献
Buck
Journal of the American Chemical Society, 1931 , vol. 53, p. 2192,2195,2198
反应条件
1: LiAlH4 2: benzene; SOCl2 View Scheme
参考文献
Barash; Osbond
Journal of the Chemical Society, 1959 , p. 2157,2163
反应条件
1: LiAlH4 2: benzene; SOCl2 View Scheme
参考文献
Barash; Osbond
Journal of the Chemical Society, 1959 , p. 2157,2163
反应条件
1: H2O 2: LiAlH4 3: benzene; SOCl2 View Scheme
参考文献
Barash; Osbond
Journal of the Chemical Society, 1959 , p. 2157,2163
反应条件
thionyl chloride; benzene
参考文献
Barash; Osbond
Journal of the Chemical Society, 1959 , p. 2157,2163
反应条件
tin(IV) chloride T=120°C;
参考文献
Lora-Tamayo et al.
Chemistry and Industry (London, United Kingdom), 1959 , p. 657
Chemische Berichte, 1960 , vol. 93, p. 289 Anm. 5
反应条件
1: NaI / ethanol 2: H2O; ethanol 3: aq. KOH / methanol View Scheme
参考文献
Sargent,L.J.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1754 - 1758
反应条件
tin(IV) chloride T=100 - 120°C;
参考文献
Lora-Tamayo et al.
Chemistry and Industry (London, United Kingdom), 1959 , p. 657
Chemische Berichte, 1960 , vol. 93, p. 289 Anm. 5
Full Text Show Details
Lora-Tamayo; Madronero
Rev.Acad.Cienc.exact.fis.nat.Madrid, 1959 , vol. 53, p. 527,543
