2-甲基-6-(4-甲基苯基)烟酸乙酯合成路线 (共 5 条)
反应条件
1: in ethanol T=50°C; Addition; 2: T=125°C; Cyclization; 1 h; Further stages.;
参考文献
Bagley, Mark C.; Bashford, Katherine E.; Hesketh, Claire L.; Moody, Christopher J.
Journal of the American Chemical Society, 2000 , vol. 122, # 14 p. 3301 - 3313
反应条件
ammonium acetate; K5CoIIIW12O40 T=115°C; 0.75 h;
参考文献
Kantevari, Srinivas; Chary, Mahankhali Venu; Vuppalapati, Srinivasu V.N.
Tetrahedron, 2007 , vol. 63, # 52 p. 13024 - 13031
反应条件
1.1: manganese dioxide / CH2Cl2 / 20 °C 2.1: ethanol / 50 °C 2.2: 100 percent / 1 h / 125 °C View Scheme
参考文献
Bagley, Mark C.; Bashford, Katherine E.; Hesketh, Claire L.; Moody, Christopher J.
Journal of the American Chemical Society, 2000 , vol. 122, # 14 p. 3301 - 3313
反应条件
1.1: 81 percent / tetrahydrofuran / 2 h / 0 °C 2.1: manganese dioxide / CH2Cl2 / 20 °C 3.1: ethanol / 50 °C 3.2: 100 percent / 1 h / 125 °C View Scheme
参考文献
Bagley, Mark C.; Bashford, Katherine E.; Hesketh, Claire L.; Moody, Christopher J.
Journal of the American Chemical Society, 2000 , vol. 122, # 14 p. 3301 - 3313
参考文献
Basu
Journal of the Indian Chemical Society, 1935 , vol. 12, p. 289,291